1-isoamyl-3-isobutylxanthine

Base Information

Chemical Name:1-isoamyl-3-isobutylxanthine
CAS No.:63908-26-9
Molecular Formula:C₁₄H₂₂N₄O₂
Molecular Weight:278.354
Hs Code.:2933990090
Mol file:63908-26-9.mol

Synonyms:1H-Purine-2,6-dione,3,7-dihydro-1-(3-methylbutyl)-3-(2-methylpropyl)- (9CI); 1-Isoamyl-3-isobutylxanthine

Suppliers and Price of 1-isoamyl-3-isobutylxanthine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 1-isoamyl-3-isobutylxanthine

Chemical Property:

Vapor Pressure:5.05E-09mmHg at 25°C
Boiling Point:470.5°Cat760mmHg
Flash Point:238.3°C
PSA：72.68000
Density:1.153g/cm³
LogP:1.58840

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1-isoamyl-3-isobutylxanthine

There total 8 articles about 1-isoamyl-3-isobutylxanthine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 94781-83-6
1-isobutyl-3-isoamyl-5-formamido-6-aminouracil

: 63908-26-9
1-isoamyl-3-isobutylxanthine

Guidance literature:: With sodium hydroxide; for 0.333333h; Heating;
DOI:10.1021/jm00382a018

Reference yield:

: 592-17-6
isobutyl urea

: 63908-26-9
1-isoamyl-3-isobutylxanthine

Guidance literature:: Multi-step reaction with 6 steps

1: 1.) acetic anhydride, 2.) 10percent NaOH / 1.) from 75 deg C to 80 deg C, 2 h, 2.) RT

2: 1.) 20percent NaOH / 1.) EtOH, 50 deg C, 2.) EtOH, reflux, 2 h

3: 79 percent / NaNO₂, 42percent AcOH / H₂O / 0.17 h / 60 °C

4: 60 percent / H₂ / PtO₂ / methanol / 0.5 h / 2068.6 Torr

5: 64 percent / 1 h / Heating

6: 87 percent / 10percent NaOH / 0.33 h / Heating

With sodium hydroxide; hydrogen; acetic anhydride; acetic acid; sodium nitrite; platinum(IV) oxide; In methanol; water;
DOI:10.1021/jm00382a018

Reference yield:

: 56075-75-3
6-amino-1-isobutyl-1,3-dihydropyrimidine-2,4-dione

: 63908-26-9
1-isoamyl-3-isobutylxanthine

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) 20percent NaOH / 1.) EtOH, 50 deg C, 2.) EtOH, reflux, 2 h

2: 79 percent / NaNO₂, 42percent AcOH / H₂O / 0.17 h / 60 °C

3: 60 percent / H₂ / PtO₂ / methanol / 0.5 h / 2068.6 Torr

4: 64 percent / 1 h / Heating

5: 87 percent / 10percent NaOH / 0.33 h / Heating

With sodium hydroxide; hydrogen; acetic acid; sodium nitrite; platinum(IV) oxide; In methanol; water;
DOI:10.1021/jm00382a018