6-methylenetestosterone acetate

Base Information

Chemical Name:6-methylenetestosterone acetate
CAS No.:1100-17-0
Molecular Formula:C₂₂H₃₀O₃
Molecular Weight:342.478
Hs Code.:
Mol file:1100-17-0.mol

Synonyms:Androst-4-en-3-one,17b-hydroxy-6-methylene-, acetate(7CI,8CI); 17b-Acetoxy-6-methyleneandrost-4-en-3-one;6-Methylenetestosterone acetate; NSC 58251

Suppliers and Price of 6-methylenetestosterone acetate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 10 raw suppliers

Chemical Property of 6-methylenetestosterone acetate

Chemical Property:

Vapor Pressure:1.18E-08mmHg at 25°C
Boiling Point:460.3°Cat760mmHg
Flash Point:199.4°C
PSA：43.37000
Density:1.11g/cm³
LogP:4.61610

Purity/Quality:: 98%,99%, ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 6-methylenetestosterone acetate

There total 16 articles about 6-methylenetestosterone acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 108-24-7
acetic anhydride

: 3347-73-7
17β-hydroxy-6-methyleneandrosta-4-ene-3-one

: 1100-17-0
6-Methylentestosteron-acetat

Guidance literature:: With pyridine; In dichloromethane; at 20 ℃; Inert atmosphere;
DOI:10.1016/j.tet.2009.06.094

Reference yield: 67.0%

: 462-95-3
formaldehyde diethyl acetal

: 1045-69-8
testosterone acetate

: 1100-17-0
6-Methylentestosteron-acetat

Guidance literature:: With sodium acetate; trichlorophosphate; In chloroform; for 1h; Heating;
DOI:10.1055/s-1982-29690

Reference yield:

: 1045-69-8
testosterone acetate

: 1100-17-0
6-Methylentestosteron-acetat

Guidance literature:: Multi-step reaction with 4 steps

1: TsOH / dioxane

2: (i) COCl₂, ClCH₂CH₂Cl, (ii) /BRN= 2628369/, Py, (iii) aq. NaOAc

3: NaBH₄ / methanol

4: aq. AcOH

With sodium tetrahydroborate; toluene-4-sulfonic acid; acetic acid; In 1,4-dioxane; methanol;
DOI:10.1016/S0040-4020(01)98622-3