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1045-69-8

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1045-69-8 Usage

Definition

ChEBI: An androstanoid that is the acetate derivative of testosterone.

Uses

An Androgen. Controlled substance.

Chemical Properties

White Solid
InChI:InChI=1/C21H30O3/c1-13(22)24-19-7-6-17-16-5-4-14-12-15(23)8-10-20(14,2)18(16)9-11-21(17,19)3/h12,16-19H,4-11H2,1-3H3

1045-69-8SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 16, 2017

Revision Date: Aug 16, 2017

1.Identification

1.1 GHS Product identifier

Product name testosterone acetate

1.2 Other means of identification

Product number -
Other names Farmatest

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only.
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:1045-69-8 SDS

1045-69-8Synthetic route

testosterone
58-22-0

testosterone

acetic anhydride
108-24-7

acetic anhydride

testosterone acetate
1045-69-8

testosterone acetate

Conditions
ConditionsYield
With pyridine; dmap at 20℃; for 24h; Inert atmosphere;100%
With pyridine at 0 - 20℃;99%
With copper(II) bis(trifluoromethanesulfonate) In dichloromethane at 20℃; for 3h;92%
testosterone
58-22-0

testosterone

acetyl chloride
75-36-5

acetyl chloride

testosterone acetate
1045-69-8

testosterone acetate

Conditions
ConditionsYield
With potassium fluoride on basic alumina In toluene for 2.5h;98%
With pyridine; acetic anhydride for 4h; Reflux;96%
With immobilized p-toluenesulfonic acid polymer bound macroporous In neat (no solvent) at 100℃; for 0.0416667h; Microwave irradiation; Sealed tube; Green chemistry;33%
With pyridine; acetic anhydride for 4h; Reflux;
androsta-4,6-dien-17β-ol-3-one acetate
2352-19-4

androsta-4,6-dien-17β-ol-3-one acetate

testosterone acetate
1045-69-8

testosterone acetate

Conditions
ConditionsYield
With palladium 10% on activated carbon; ammonium formate In ethanol at 75 - 77℃; for 9.5h; Inert atmosphere;97.6%
17β-Acetoxytestosterone tosylhydrazone

17β-Acetoxytestosterone tosylhydrazone

A

testosterone acetate
1045-69-8

testosterone acetate

B

17β-Acetoxy-4α,5-epoxyandrostan-3-one

17β-Acetoxy-4α,5-epoxyandrostan-3-one

Conditions
ConditionsYield
With 3,3-dimethyldioxirane In acetone at 20℃; for 1h; Yields of byproduct given;A 95%
B n/a
17β-acetoxy-4,5-epoxy-5β-androstan-3-one
2944-75-4

17β-acetoxy-4,5-epoxy-5β-androstan-3-one

testosterone acetate
1045-69-8

testosterone acetate

Conditions
ConditionsYield
With Amberlyst 15; sodium iodide In acetone at 20℃; for 6h; deoxygenation;95%
testosterone
58-22-0

testosterone

acetic acid
64-19-7

acetic acid

testosterone acetate
1045-69-8

testosterone acetate

Conditions
ConditionsYield
Stage #1: acetic acid With benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide In chloroform at 20℃; for 0.5h; Inert atmosphere;
Stage #2: testosterone With dmap In chloroform for 18h; Inert atmosphere; Reflux;
95%
testosterone
58-22-0

testosterone

ethyl acetate
141-78-6

ethyl acetate

testosterone acetate
1045-69-8

testosterone acetate

Conditions
ConditionsYield
With C12F18O13Zn4 for 40h; Reflux; Inert atmosphere;93%
17β-acetoxyandrost-4-ene
6157-79-5

17β-acetoxyandrost-4-ene

testosterone acetate
1045-69-8

testosterone acetate

Conditions
ConditionsYield
With tert.-butylhydroperoxide; cobalt(II) acetate In decane; acetonitrile at 55℃; for 3h;70%
acetic anhydride
108-24-7

acetic anhydride

17β-<(t-butyldimethylsilyl)oxy>androst-4-en-3-one
57711-43-0

17β-<(t-butyldimethylsilyl)oxy>androst-4-en-3-one

testosterone acetate
1045-69-8

testosterone acetate

Conditions
ConditionsYield
copper(II) bis(trifluoromethanesulfonate) In dichloromethane at 20℃; for 24h;67%
Acetic acid (2S,8R,9S,10R,13S,14S,17S)-4-bromo-10,13-dimethyl-2-morpholin-4-yl-3-oxo-2,3,6,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-17-yl ester
105360-48-3

Acetic acid (2S,8R,9S,10R,13S,14S,17S)-4-bromo-10,13-dimethyl-2-morpholin-4-yl-3-oxo-2,3,6,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-17-yl ester

A

testosterone acetate
1045-69-8

testosterone acetate

B

17β-acetoxy-4-bromo-4-androsten-3-one
21002-81-3

17β-acetoxy-4-bromo-4-androsten-3-one

Conditions
ConditionsYield
With zinc In acetic acid at 25℃; for 15h;A 30%
B 64%
testosterone
58-22-0

testosterone

acetic acid
64-19-7

acetic acid

A

di(4-methyl)phenylthiosulfonate
2943-42-2

di(4-methyl)phenylthiosulfonate

B

testosterone acetate
1045-69-8

testosterone acetate

C

(9S,10R,13S,14S)-10,13-dimethyl-3-oxo-2,3,6,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-17-yl 4-methylbenzenesulfinate
81917-15-9

(9S,10R,13S,14S)-10,13-dimethyl-3-oxo-2,3,6,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-17-yl 4-methylbenzenesulfinate

Conditions
ConditionsYield
With p-toluene sulfinic acid In dichloromethane for 24h; Ambient temperature;A 20 mg
B 60%
C 10 mg
/PBOND001-1390/

/PBOND001-1390/

A

testosterone acetate
1045-69-8

testosterone acetate

B

17β-acetoxy-4,5-secoandrostane-3,5-dione
98735-19-4

17β-acetoxy-4,5-secoandrostane-3,5-dione

Conditions
ConditionsYield
With zinc In acetic acid for 12h; Heating; Yields of byproduct given;A 44%
B n/a
With zinc In acetic acid for 12h; Heating; Yield given;A 44%
B n/a
17β-acetoxy-androsta-1,4-dien-3-one
2363-59-9

17β-acetoxy-androsta-1,4-dien-3-one

testosterone acetate
1045-69-8

testosterone acetate

Conditions
ConditionsYield
With thallium(III) nitrate trihydrate In diethylene glycol dimethyl ether for 24h; Ambient temperature;34%
17β-acetoxy-3-ethoxy-androsta-3,5-diene
52091-98-2

17β-acetoxy-3-ethoxy-androsta-3,5-diene

testosterone acetate
1045-69-8

testosterone acetate

Conditions
ConditionsYield
With hydrogenchloride; acetone
With hydrogenchloride; acetone
17β-acetoxy-3β-formyloxy-androst-5-ene
111294-86-1

17β-acetoxy-3β-formyloxy-androst-5-ene

testosterone acetate
1045-69-8

testosterone acetate

17β-acetoxy-3β-cyclohex-1-enyloxy-androst-5-ene

17β-acetoxy-3β-cyclohex-1-enyloxy-androst-5-ene

testosterone acetate
1045-69-8

testosterone acetate

3β.3'β-dihydroxy-17β.17β'-diacetoxy-[3.3']bi[androsten-(4)-yl]
97922-54-8

3β.3'β-dihydroxy-17β.17β'-diacetoxy-[3.3']bi[androsten-(4)-yl]

testosterone acetate
1045-69-8

testosterone acetate

Conditions
ConditionsYield
With chloroform; bromine Behandeln des Reaktionsprodukts mit CrO3 in wasserhaltiger Essigsaeure und Aether und Schuetteln des danach erhaltenen Reaktionsprodukts mit Zink-Pulver und wss.Essigsaeure;
17-chloroandrost-4-en-3-one
911651-92-8

17-chloroandrost-4-en-3-one

potassium acetate
127-08-2

potassium acetate

testosterone acetate
1045-69-8

testosterone acetate

Conditions
ConditionsYield
With acetic acid at 180℃;
androstenediol-17-acetate
5937-72-4

androstenediol-17-acetate

testosterone acetate
1045-69-8

testosterone acetate

Conditions
ConditionsYield
With aluminum tri-tert-butoxide; acetone; toluene
With bromine; acetic acid nachfolgendes Erwaermen mit CrO3 in Essigsaeure und Erwaermen des Reaktionsprodukts mit Zink-Pulver und Essigsaeure;
With bromine; acetic acid nachfolgendes Erwaermen mit CrO3 in Essigsaeure und Erwaermen des Reaktionsprodukts mit NaI in Aethanol;
testosterone
58-22-0

testosterone

acetic anhydride
108-24-7

acetic anhydride

toluene
108-88-3

toluene

testosterone acetate
1045-69-8

testosterone acetate

17-chloroandrost-4-en-3-one
911651-92-8

17-chloroandrost-4-en-3-one

potassium acetate
127-08-2

potassium acetate

acetic acid
64-19-7

acetic acid

testosterone acetate
1045-69-8

testosterone acetate

Conditions
ConditionsYield
at 150 - 180℃;
androstenediol-17-acetate
5937-72-4

androstenediol-17-acetate

aluminum tri-tert-butoxide
556-91-2

aluminum tri-tert-butoxide

acetone
67-64-1

acetone

toluene
108-88-3

toluene

testosterone acetate
1045-69-8

testosterone acetate

androstenediol-17-acetate
5937-72-4

androstenediol-17-acetate

aluminum tri-tert-butoxide
556-91-2

aluminum tri-tert-butoxide

acetone
67-64-1

acetone

benzene
71-43-2

benzene

testosterone acetate
1045-69-8

testosterone acetate

Progesterone
57-83-0

Progesterone

A

17-hydroxyprogesterone
68-96-2

17-hydroxyprogesterone

B

testosterone acetate
1045-69-8

testosterone acetate

Conditions
ConditionsYield
With potassium phosphate; 1,2-dilauroylphosphatidylcholine; NADPH; magnesium chloride Mechanism; microsomes from pig tests, CYP-17, cytochrome P450 reductase;
17β-acetoxy-4-oxa-androst-5-en-3-one
1458-92-0

17β-acetoxy-4-oxa-androst-5-en-3-one

acetic acid
64-19-7

acetic acid

dimethyl methane phosphonate
756-79-6

dimethyl methane phosphonate

A

testosterone
58-22-0

testosterone

B

testosterone acetate
1045-69-8

testosterone acetate

Conditions
ConditionsYield
Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
17β-acetoxy-4-oxa-androst-5-en-3-one
1458-92-0

17β-acetoxy-4-oxa-androst-5-en-3-one

dimethyl methane phosphonate
756-79-6

dimethyl methane phosphonate

A

testosterone
58-22-0

testosterone

B

testosterone acetate
1045-69-8

testosterone acetate

Conditions
ConditionsYield
Yield given. Multistep reaction. Yields of byproduct given;
Progesterone
57-83-0

Progesterone

A

testosterone acetate
1045-69-8

testosterone acetate

B

6β,11α-dihydroxyprogesterone
600-48-6

6β,11α-dihydroxyprogesterone

C

12β,17α-dihydroxyprogesterone
604-03-5

12β,17α-dihydroxyprogesterone

D

6β,11α,20(R)-trihydroxypregna-4-en-3-one

6β,11α,20(R)-trihydroxypregna-4-en-3-one

Conditions
ConditionsYield
With Cephalosporium aphidicola In ethanol for 168h;A 33 mg
B 1.1 g
C 39 mg
D 41 mg
Progesterone
57-83-0

Progesterone

A

testosterone
58-22-0

testosterone

B

pregna-1,4-diene-3,20-dione
1162-54-5

pregna-1,4-diene-3,20-dione

C

Androstenedione
63-05-8

Androstenedione

D

testosterone acetate
1045-69-8

testosterone acetate

E

11-alpha-hydroxyprogesterone
80-75-1

11-alpha-hydroxyprogesterone

F

1-dehydrotestosterone
846-48-0

1-dehydrotestosterone

Conditions
ConditionsYield
With immobilized spores of Aspergillus ochraceus; Tris-maleate buffer at 30℃; for 48h; Product distribution; Mechanism; various water activity of the biocatalysts;
17β-acetoxy-3α,4α-epoxy-5α-hydroxyandrostane
209853-71-4

17β-acetoxy-3α,4α-epoxy-5α-hydroxyandrostane

A

testosterone acetate
1045-69-8

testosterone acetate

B

17β-acetoxy-4-methylestra-1,3,5(10)-triene
798-35-6

17β-acetoxy-4-methylestra-1,3,5(10)-triene

C

17β-acetyloxy-5α-androst-2-en-4-one
65-01-0

17β-acetyloxy-5α-androst-2-en-4-one

Conditions
ConditionsYield
With hydrogen bromide; acetic acid for 0.25h; Rearrangement; Heating;A 15 mg
B 29 mg
C 10 mg
testosterone acetate
1045-69-8

testosterone acetate

17β-acetoxyandrost-4-ene
6157-79-5

17β-acetoxyandrost-4-ene

Conditions
ConditionsYield
With sodium tetrahydroborate; acetic acid; trifluoroacetic acid In dichloromethane; acetonitrile at 20℃; for 3.5h; Inert atmosphere;99%
With sodium tetrahydroborate; acetic acid; trifluoroacetic acid In dichloromethane; acetonitrile at 0℃; for 10h;80%
(i) EtSH, HCl, Et2O, (ii) Raney-Ni, dioxane; Multistep reaction;
With sodium tetrahydroborate; acetic acid; trifluoroacetic acid In dichloromethane; acetonitrile for 1h; Ambient temperature;2.2 g
testosterone acetate
1045-69-8

testosterone acetate

(3β,17β)-3-hydroxyandrost-4-en-17-yl acetate
16992-89-5, 17320-63-7, 95119-10-1, 13903-65-6

(3β,17β)-3-hydroxyandrost-4-en-17-yl acetate

Conditions
ConditionsYield
With methanol; sodium tetrahydroborate In tetrahydrofuran at 0℃;97.3%
With sodium tetrahydroborate In methanol at 0℃; for 2h;74%
With sodium tetrahydroborate In methanol at 0℃; for 2h;
With lithium tri-(tert-butoxy)aluminum hydride In tetrahydrofuran for 3.5h; Inert atmosphere; Reflux;
testosterone acetate
1045-69-8

testosterone acetate

17β-acetoxy-5β-androstan-3-one
1164-92-7

17β-acetoxy-5β-androstan-3-one

Conditions
ConditionsYield
With hydrogen; palladium In pyridine for 16h;97%
Multi-step reaction with 2 steps
1: H2 / PtO2 / acetic acid / 1 h / Ambient temperature
2: Jones reagent / acetone / 0.08 h
View Scheme
testosterone acetate
1045-69-8

testosterone acetate

17β-acetoxy-4-bromo-4-androsten-3-one
21002-81-3

17β-acetoxy-4-bromo-4-androsten-3-one

Conditions
ConditionsYield
Stage #1: testosterone acetate With 3,3-dimethyldioxirane In acetone at 20℃; for 8h; Epoxidation;
Stage #2: With Amberlyst 15; sodium bromide In acetone at 20℃; for 12h; Bromination;
97%
testosterone acetate
1045-69-8

testosterone acetate

testosterone
58-22-0

testosterone

Conditions
ConditionsYield
With copper dichloride In methanol; water for 20h; Heating;95%
With bis(tri-n-butyltin)oxide In toluene at 110℃; for 27h;59%
With potassium hydroxide
pyrrolidine
123-75-1

pyrrolidine

testosterone acetate
1045-69-8

testosterone acetate

3-(1-pyrrolidinyl)-17β-acetoxyandrosta-3,5-diene
22234-09-9

3-(1-pyrrolidinyl)-17β-acetoxyandrosta-3,5-diene

Conditions
ConditionsYield
92%
In methanol Heating;84%
testosterone acetate
1045-69-8

testosterone acetate

clostebol acetate
855-19-6

clostebol acetate

Conditions
ConditionsYield
Stage #1: testosterone acetate With 3,3-dimethyldioxirane In acetone at 20℃; for 8h; Epoxidation;
Stage #2: With Amberlyst 15; sodium chloride In acetone at 20℃; for 12h; Chlorination;
89%
With pyridine; sulfuryl dichloride for 1h; Product distribution; Ambient temperature; other steroids;
With pyridine; sulfuryl dichloride for 1h; Ambient temperature;
Multi-step reaction with 2 steps
1: N-chloro-succinimide, HN3 / CHCl3; 2-methyl-propan-2-ol
2: SiO2 / benzene
View Scheme
Multi-step reaction with 2 steps
1: N-chloro-succinimide, HN3 / CHCl3; 2-methyl-propan-2-ol
2: SiO2 / benzene
View Scheme
testosterone acetate
1045-69-8

testosterone acetate

3-((3S,3aS,5aS,6R,9aS,9bS)-3-acetoxy-3a,6-dimethyl-7-oxododecahydro-1H-cyclopenta[a]naphthalen-6-yl)propanoic acid
7430-16-2

3-((3S,3aS,5aS,6R,9aS,9bS)-3-acetoxy-3a,6-dimethyl-7-oxododecahydro-1H-cyclopenta[a]naphthalen-6-yl)propanoic acid

Conditions
ConditionsYield
With potassium permanganate; sodium periodate; sodium carbonate In water; tert-butyl alcohol at 70℃; for 0.333333h; Inert atmosphere;88%
With potassium permanganate; potassium metaperiodate; potassium carbonate In water; tert-butyl alcohol for 2h;76%
With potassium permanganate; sodium periodate; sodium carbonate In water; isopropyl alcohol for 1h; Heating;
testosterone acetate
1045-69-8

testosterone acetate

2-phenylcinchoninoylhydrazide

2-phenylcinchoninoylhydrazide

Acetic acid (8R,9S,10R,13S,14S,17S)-10,13-dimethyl-3-[(2-phenyl-quinoline-5-carbonyl)-hydrazono]-2,3,6,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-17-yl ester
74996-51-3

Acetic acid (8R,9S,10R,13S,14S,17S)-10,13-dimethyl-3-[(2-phenyl-quinoline-5-carbonyl)-hydrazono]-2,3,6,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-17-yl ester

Conditions
ConditionsYield
With pyridine In ethanol for 40h; Heating;87%
isoniazid
54-85-3

isoniazid

testosterone acetate
1045-69-8

testosterone acetate

Acetic acid (8R,9S,10R,13S,14S,17S)-10,13-dimethyl-3-[(pyridine-4-carbonyl)-hydrazono]-2,3,6,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-17-yl ester
74996-50-2

Acetic acid (8R,9S,10R,13S,14S,17S)-10,13-dimethyl-3-[(pyridine-4-carbonyl)-hydrazono]-2,3,6,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-17-yl ester

Conditions
ConditionsYield
With pyridine In ethanol for 25h; Heating;86%
testosterone acetate
1045-69-8

testosterone acetate

ethylenediamine
107-15-3

ethylenediamine

17β-acetoxy-4'-dehydro-androst-4-eno[3,4-e]piperazin-6-one
1104455-80-2

17β-acetoxy-4'-dehydro-androst-4-eno[3,4-e]piperazin-6-one

Conditions
ConditionsYield
With aluminum oxide at 120℃; microwave irradiation;85%
testosterone acetate
1045-69-8

testosterone acetate

manganese triacetate

manganese triacetate

Δ4-Androsten-2,17-diol-3-on-diacetat
95720-22-2

Δ4-Androsten-2,17-diol-3-on-diacetat

Conditions
ConditionsYield
In benzene at 80℃; for 25h;83%
testosterone acetate
1045-69-8

testosterone acetate

Nα-<1,2-bis(p-methoxyphenyl)butyl>-α-aminoacetohydrazide
77579-59-0

Nα-<1,2-bis(p-methoxyphenyl)butyl>-α-aminoacetohydrazide

Acetic acid (8R,9S,10R,13S,14S,17S)-3-({2-[1,2-bis-(4-methoxy-phenyl)-butylamino]-acetyl}-hydrazono)-10,13-dimethyl-2,3,6,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-17-yl ester
77579-64-7

Acetic acid (8R,9S,10R,13S,14S,17S)-3-({2-[1,2-bis-(4-methoxy-phenyl)-butylamino]-acetyl}-hydrazono)-10,13-dimethyl-2,3,6,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-17-yl ester

Conditions
ConditionsYield
With acetic acid In ethanol Heating;80%
testosterone acetate
1045-69-8

testosterone acetate

methylmagnesium bromide
75-16-1

methylmagnesium bromide

17β-acetoxy-3β-hydroxy-3α-methylandrost-4-ene

17β-acetoxy-3β-hydroxy-3α-methylandrost-4-ene

Conditions
ConditionsYield
In tetrahydrofuran; diethyl ether Grignard reaction;76%
morpholine
110-91-8

morpholine

testosterone acetate
1045-69-8

testosterone acetate

3-morpholinoandrosta-2,5-dein-17β-yl acetate
84736-46-9

3-morpholinoandrosta-2,5-dein-17β-yl acetate

Conditions
ConditionsYield
With toluene-4-sulfonic acid In toluene for 16h; Heating;75%
methanol
67-56-1

methanol

testosterone acetate
1045-69-8

testosterone acetate

A-nor-2α-methoxycarbonyl-3-androsten-17β-yl acetate
77579-50-1

A-nor-2α-methoxycarbonyl-3-androsten-17β-yl acetate

Conditions
ConditionsYield
With thallium(III) nitrate; trimethyl orthoformate for 0.5h;75%
testosterone acetate
1045-69-8

testosterone acetate

trimethyl orthoformate
149-73-5

trimethyl orthoformate

A-nor-2α-methoxycarbonyl-3-androsten-17β-yl acetate
77579-50-1

A-nor-2α-methoxycarbonyl-3-androsten-17β-yl acetate

Conditions
ConditionsYield
With thallium(III) nitrate In methanol at 0℃; for 0.5h;75%
testosterone acetate
1045-69-8

testosterone acetate

17β-acetoxy-3-hydroximinoandrost-4-ene
59285-18-6

17β-acetoxy-3-hydroximinoandrost-4-ene

Conditions
ConditionsYield
With pyridine; hydroxylamine hydrochloride for 6h; Reflux;74%
testosterone acetate
1045-69-8

testosterone acetate

17β-hydroxyandrost-5-en-3-one
571-25-5

17β-hydroxyandrost-5-en-3-one

Conditions
ConditionsYield
With potassium hydroxide; sodium hydrogencarbonate; acetic acid In 1,2-dimethoxyethane for 15h; Ambient temperature;70%
testosterone acetate
1045-69-8

testosterone acetate

4-aminobenzohydrazide
5351-17-7

4-aminobenzohydrazide

Acetic acid (8R,9S,10R,13S,14S,17S)-3-[(4-amino-benzoyl)-hydrazono]-10,13-dimethyl-2,3,6,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-17-yl ester
74996-49-9

Acetic acid (8R,9S,10R,13S,14S,17S)-3-[(4-amino-benzoyl)-hydrazono]-10,13-dimethyl-2,3,6,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-17-yl ester

Conditions
ConditionsYield
With pyridine In ethanol for 25h; Heating;70%
testosterone acetate
1045-69-8

testosterone acetate

stanolone acetate
1164-91-6

stanolone acetate

Conditions
ConditionsYield
With potato dextrose broth medium In ethanol at 24 - 26℃; for 96h; Penicillium decumbens ATCC 10436;68%
Multi-step reaction with 2 steps
1: H2 / PtO2 / acetic acid / 1 h / Ambient temperature
2: Jones reagent / acetone / 0.08 h
View Scheme
testosterone acetate
1045-69-8

testosterone acetate

17beta-Acetoxyandrost-4-ene-3,6-dione
4594-27-8, 6726-17-6

17beta-Acetoxyandrost-4-ene-3,6-dione

Conditions
ConditionsYield
With tert.-butylhydroperoxide; Rh2(cap)4 In water at 40℃; for 16h; Product distribution / selectivity; Allylic oxidation;68%
With tert.-butylhydroperoxide; [Rh2(cap)4*2CH3CN] In water at 40℃; for 48h;68%
With tert.-butylhydroperoxide; Rh2(cap)4 In 1,2-dichloro-ethane at 40℃; for 16h; Product distribution / selectivity; Allylic oxidation;50%
With tert.-butylhydroperoxide; Clorox bleach
Multi-step reaction with 2 steps
1: TsOH / dioxane
2: (tBuO)2CrO2 / CCl4
View Scheme

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