2-chloro-N-propylbenzamide

Base Information

Chemical Name:2-chloro-N-propylbenzamide
CAS No.:66896-67-1
Molecular Formula:C10H12ClNO
Molecular Weight:197.6614
Hs Code.:2924299090
NSC Number:405483
DSSTox Substance ID:DTXSID60324012
Wikidata:Q82083378

Synonyms:2-chloro-N-propylbenzamide;66896-67-1;2-Chloro-N-n-propylbenzamide;2-chloro-N-propyl-benzamide;NSC405483;starbld0004434;Benzamide, 2-chloro-N-propyl-;SCHEMBL10792384;DTXSID60324012;MFCD01212176;STL071224;AKOS000499867;NSC 405483;NSC-405483;AN-329/11634105

Suppliers and Price of 2-chloro-N-propylbenzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of 2-chloro-N-propylbenzamide

Chemical Property:

Vapor Pressure:0.000262mmHg at 25°C
Boiling Point:323.4°Cat760mmHg
Flash Point:149.4°C
PSA：29.10000
Density:1.131g/cm³
LogP:2.87070
XLogP3:1.8
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:3
Exact Mass:197.0607417
Heavy Atom Count:13
Complexity:172

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCNC(=O)C1=CC=CC=C1Cl

Technology Process of 2-chloro-N-propylbenzamide

There total 3 articles about 2-chloro-N-propylbenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 10546-70-0
N-(n-propyl)benzamide

: 66896-67-1
2-chloro-N-propylbenzamide

Guidance literature:: With sodium persulfate; N-chloro-succinimide; trifluorormethanesulfonic acid; palladium diacetate; In 1,2-dichloro-ethane; at 80 ℃; for 7h; regioselective reaction; Sealed tube;
DOI:10.1002/anie.201300176

Reference yield: 62.0%

: 107-10-8,42939-71-9
propylamine

: 873-31-4
2-chlorophenylacetylene

: 66896-67-1
2-chloro-N-propylbenzamide

Guidance literature:: 2-chlorophenylacetylene; With [bis(acetoxy)iodo]benzene; water; sodium hydrogencarbonate; at 20 ℃; for 1h;

propylamine; at 20 ℃; for 3.5h;
DOI:10.1039/c4cc07961b

Reference yield: 46.0%

: 107-10-8,42939-71-9
propylamine

: 89-98-5
2-chloro-benzaldehyde

: 66896-67-1
2-chloro-N-propylbenzamide

Guidance literature:: With [bis(acetoxy)iodo]benzene; water; In chloroform; at 0 - 20 ℃; for 20h; Inert atmosphere;
DOI:10.1055/s-2008-1078218