55DIAMINO22DIMETHYLAZOXYBENZENE

Base Information

• Chemical Name: 55DIAMINO22DIMETHYLAZOXYBENZENE
• CAS No.: 138805-30-8
• Molecular Formula: C14H16 N4 O
• Molecular Weight: 256.307
• Mol file: 138805-30-8.mol

Synonyms:55DIAMINO22DIMETHYLAZOXYBENZENE

Chemical Property of 55DIAMINO22DIMETHYLAZOXYBENZENE

Chemical Property:

• Vapor Pressure: 3.8E-11mmHg at 25°C
• Boiling Point: 525.8°C at 760 mmHg
• Flash Point: 271.8°C
• PSA: 93.15000
• Density: 1.24g/cm³
• LogP: 5.07910

Purity/Quality:

Safty Information:

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MSDS Files:

SDS file from LookChem

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Technology Process of 55DIAMINO22DIMETHYLAZOXYBENZENE

There total 6 articles about 55DIAMINO22DIMETHYLAZOXYBENZENE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.3%

4-methylbenzene-1,3-diamine (95-80-7,71111-07-4) → 4,4'-dimethyl-3,3'-azoxy-di-aniline (138805-30-8)

Guidance literature:

With Novozym 435; urea hydrogen peroxide adduct; ethyl acetate; at 20 ℃; for 1h; Enzymatic reaction;

DOI:10.1002/cctc.201500720

Reference yield:

4-Methyl-3-nitroanilin (119-32-4) → 4-methylbenzene-1,3-diamine (95-80-7,71111-07-4) + 4,4'-dimethyl-3,3'-azoxy-di-aniline (138805-30-8) + (E)-3,3'-(diazene-1,2-diyl)bis(4-methylaniline) (138805-29-5) + N,N'-bis-(5-amino-2-methyl-phenyl)-hydrazine

Guidance literature:

bei der elektrolytischen Reduktion, je nach der zugefuehrten Strommenge Produkt 2, 3 oder 4 entsteht;

Reference yield:

4-Methyl-3-nitroanilin (119-32-4) → 4,4'-dimethyl-3,3'-azoxy-di-aniline (138805-30-8)

Guidance literature:

With sodium amalgam; ethanol;

upstream raw materials:

4-Methyl-3-nitroanilin

ethanol

4-methylbenzene-1,3-diamine

Downstream raw materials:

(E)-3,3'-(diazene-1,2-diyl)bis(4-methylaniline)

bis-(5-acetylamino-2-methyl-phenyl)-diazene-N-oxide

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