4-Nitrodiazoaminobenzene

Base Information

• Chemical Name: 4-Nitrodiazoaminobenzene
• CAS No.: 13113-75-2
• Molecular Formula: C12H10 N4 O2
• Molecular Weight: 242.237
• Hs Code.: 2928000090
• European Community (EC) Number: 678-263-1
• NSC Number: 69814
• DSSTox Substance ID: DTXSID80290588
• Nikkaji Number: J208.772C
• ChEMBL ID: CHEMBL1544497
• Mol file: 13113-75-2.mol

Synonyms:4-Nitrodiazoaminobenzene;13113-75-2;N-[(4-nitrophenyl)diazenyl]aniline;p-Nitrodiazoaminobenzene;1-(4-Nitrophenyl)-3-phenyltriazene;(1e)-1-(4-nitrophenyl)-3-phenyltriaz-1-ene;p-(Nitrodiazoamino)azobenzene;Triazene, 1-(p-nitrophenyl)-3-phenyl-;MLS000719986;1-Triazene, 1-(4-nitrophenyl)-3-phenyl-;SMR000304515;1-Triazene, 3-(4-nitrophenyl)-1-phenyl-;(1E)-3-(4-nitrophenyl)-1-phenyltriaz-1-ene;NSC69814;4-Nitrodiazoaminobenzol;N-(4-nitrophenyl)azoaniline;cid_250380;SCHEMBL2842727;(4-nitrophenyl)azo-phenyl-amine;CHEMBL1544497;BDBM76544;Aniline, N-(4-nitrophenylazo)-;DTXSID80290588;VPLPKIVQGJVXDR-UHFFFAOYSA-N;HMS2601O03;NSC-69814;STK180719;AKOS001572749;AKOS022180711;1-(4-Nitrophenyl)-3-phenyltriaz-1-ene;FT-0755856;N0189;(E)-1-(4-nitrophenyl)-3-phenyltriaz-1-ene;(1E)-1-(4-Nitrophenyl)-3-phenyl-1-triazene #;SR-01000106136;SR-01000106136-1

Chemical Property of 4-Nitrodiazoaminobenzene

Chemical Property:

• Vapor Pressure: 1.6E-06mmHg at 25°C
• Melting Point: 137 °C
• Boiling Point: 397.3°Cat760mmHg
• PKA: 0.43±0.50(Predicted)
• Flash Point: 194.1°C
• PSA: 82.57000
• Density: 1.28g/cm³
• LogP: 4.30180
• XLogP3: 3.8
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 5
• Rotatable Bond Count: 3
• Exact Mass: 242.08037557
• Heavy Atom Count: 18
• Complexity: 289

Purity/Quality:

98%,99%, ^*data from raw suppliers

4-NITRODIAZOAMINOBENZENE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C=C1)NN=NC2=CC=C(C=C2)[N+](=O)[O-]

Technology Process of 4-Nitrodiazoaminobenzene

There total 8 articles about 4-Nitrodiazoaminobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

p-nitrophenylazobenzenethiosulfonate (91363-26-7) + aniline (62-53-3) → p-nitrophenylbenzotriazene (13113-75-2)

Guidance literature:

at 30 - 50 ℃; for 2.5h;

Reference yield:

4-nitro-aniline (100-01-6,104810-17-5) → p-nitrophenylbenzotriazene (13113-75-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) NaNO₂, aq. HCl, 2.) NaHCO₃ / 2.) -5 - -3 deg C

2: 81 percent / 2.5 h / 30 - 50 °C

With hydrogenchloride; sodium hydrogencarbonate; sodium nitrite;

Reference yield:

p-nitrobenzenediazonium (14368-49-1) + aniline (62-53-3) → p-nitrophenylbenzotriazene (13113-75-2)

Guidance literature:

With sodium acetate;

upstream raw materials:

p-nitrobenzenediazonium

aniline

4-nitrobenzenediazonium chloride

sodium acetate

Downstream raw materials:

4-nitro-aniline

aniline yellow

disperse orange 3

phenol

Refernces