N-(2-Hydroxyethyl)-4-cyclohexene-1,2-dicarboximide

Base Information

Chemical Name:N-(2-Hydroxyethyl)-4-cyclohexene-1,2-dicarboximide
CAS No.:15458-48-7
Molecular Formula:C₁₀H₁₃NO₃
Molecular Weight:195.218
Hs Code.:
European Community (EC) Number:239-477-7
NSC Number:68479
DSSTox Substance ID:DTXSID70935017
Nikkaji Number:J26.861E
Mol file:15458-48-7.mol

Synonyms:n-(2-hydroxyethyl)-1,2,3,6-tetrahydrophthalimide;15458-48-7;N-(2-Hydroxyethyl)-4-cyclohexene-1,2-dicarboximide;2-(2-hydroxyethyl)-3a,4,7,7a-tetrahydroisoindole-1,3-dione;EINECS 239-477-7;AI3-07478;EC 239-477-7;N-(2-Hydroxyethyl)-1,2,3,6-tetrahydrophihalimide;1,2,3,6,-Tetrahydro-N-(2-hydroxyethyl)phthalimide;N-(.beta.-Hydroxyethyl)-4-cyclohexen-1,2-dicarboximide;1H-Isoindole-1,3(2H)-dione, 3a,4,7,7a-tetrahydro-2-(2-hydroxyethyl)-;2-(2-Hydroxyethyl)-3a,4,7,7a-tetrahydro-1H-isoindole-1,3(2H)-dione;SCHEMBL5878378;DTXSID70935017;NSC68479;MFCD00043550;NSC 68479;NSC-68479;AKOS009552238;FT-0629138;N-(.beta.-Hydroxyethyl)-4-cyclohexene-1,2-dicarboximide;2-(2-Hydroxyethyl)-3a,4,7,7a-tetrahydro-1H-isoindole-1,3(2H)-dione #

Suppliers and Price of N-(2-Hydroxyethyl)-4-cyclohexene-1,2-dicarboximide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Matrix Scientific
N-(2-Hydroxyethyl)-4-cyclohexene-1,2-dicarboximide
1g
$ 82.00

American Custom Chemicals Corporation
N-(2-HYDROXYETHYL)-4-CYCLOHEXENE-1,2-DICARBOXIMIDE 95.00%
1G
$ 660.95

Total 11 raw suppliers

Chemical Property of N-(2-Hydroxyethyl)-4-cyclohexene-1,2-dicarboximide

Chemical Property:

Vapor Pressure:3.72E-08mmHg at 25°C
Boiling Point:402.6°Cat760mmHg
Flash Point:197.3°C
PSA：57.61000
Density:1.274g/cm³
LogP:-0.13220
XLogP3:0.3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:195.08954328
Heavy Atom Count:14
Complexity:272

Purity/Quality:

99.9% ^*data from raw suppliers

N-(2-Hydroxyethyl)-4-cyclohexene-1,2-dicarboximide ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1C=CCC2C1C(=O)N(C2=O)CCO

Technology Process of N-(2-Hydroxyethyl)-4-cyclohexene-1,2-dicarboximide

There total 2 articles about N-(2-Hydroxyethyl)-4-cyclohexene-1,2-dicarboximide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 141-43-5
ethanolamine

: 935-79-5
cis-1,2,3,6-tetrahydrophthalic anhydride

: 38772-50-8,15458-48-7
(3aR,7aS)-2-(2-hydroxyethyl)-3a,4,7,7a-tetrahydro-1H-isoindole-1,3(2H)-dione

Guidance literature:: In neat (no solvent); at 130 ℃;
DOI:10.1039/c6sc05627j

Reference yield:

: 38772-50-8,15458-48-7
(3aR,7aS)-2-(2-hydroxyethyl)-3a,4,7,7a-tetrahydro-1H-isoindole-1,3(2H)-dione

Guidance literature:: Anhydrid-cis-cyclohexen-(4)-dicarbonsaeure-(1,2), 2-Amino-ethanol-(1);

Reference yield:

: 38772-50-8,15458-48-7
(3aR,7aS)-2-(2-hydroxyethyl)-3a,4,7,7a-tetrahydro-1H-isoindole-1,3(2H)-dione

: C₁₉H₂₂INO₃

Guidance literature:: Multi-step reaction with 3 steps

1: trifluorormethanesulfonic acid / dichloromethane

2: sodium hydride / N,N-dimethyl-formamide

3: tetrabutyl ammonium fluoride / tetrahydrofuran

With trifluorormethanesulfonic acid; tetrabutyl ammonium fluoride; sodium hydride; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c6sc05627j