7-Chloro-2-p-tolyl-benzo[d][1,3]oxazin-4-one

Base Information

Chemical Name:7-Chloro-2-p-tolyl-benzo[d][1,3]oxazin-4-one
CAS No.:40728-69-6
Molecular Formula:C15H10ClNO2
Molecular Weight:271.6984
Hs Code.:
NSC Number:159061
DSSTox Substance ID:DTXSID80303561
Nikkaji Number:J1.272.980D
Wikidata:Q82048913
Mol file:40728-69-6.mol

Synonyms:7-Chloro-2-p-tolyl-benzo[d][1,3]oxazin-4-one;40728-69-6;7-chloro-2-(4-methylphenyl)-3,1-benzoxazin-4-one;7-chloro-2-(4-methylphenyl)-4H-3,1-benzoxazin-4-one;NSC159061;DTXSID80303561;STK224241;AKOS000642633;CCG-324180;NSC-159061

Suppliers and Price of 7-Chloro-2-p-tolyl-benzo[d][1,3]oxazin-4-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 7-Chloro-2-p-tolyl-benzo[d][1,3]oxazin-4-one

Chemical Property:

Vapor Pressure:1.33E-06mmHg at 25°C
Boiling Point:399.9°Cat760mmHg
Flash Point:195.6°C
PSA：43.10000
Density:1.32g/cm³
LogP:3.81680
XLogP3:3.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:1
Exact Mass:271.0400063
Heavy Atom Count:19
Complexity:388

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=C(C=C1)C2=NC3=C(C=CC(=C3)Cl)C(=O)O2

Technology Process of 7-Chloro-2-p-tolyl-benzo[d][1,3]oxazin-4-one

There total 7 articles about 7-Chloro-2-p-tolyl-benzo[d][1,3]oxazin-4-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 874-60-2
4-methyl-benzoyl chloride

: 89-77-0
2-Amino-4-chlorobenzoic acid

: 40728-69-6
7-chloro-2-(p-tolyl)-4H-benzo[d][1,3]oxazin-4-one

Guidance literature:: With pyridine; for 0.5h;
DOI:10.1016/S1386-1425(99)00206-1

Reference yield: 85.0%

: C₁₅H₁₀ClN₃O₃

: 40728-69-6
7-chloro-2-(p-tolyl)-4H-benzo[d][1,3]oxazin-4-one

Guidance literature:: With 1,1,3,3-Tetramethyldisiloxane; copper(II) bis(trifluoromethanesulfonate); triphenylphosphine; In toluene; Reflux;
DOI:10.1021/acscatal.6b00165

Reference yield: 59.0%

: benzene-1,3,5-triyl triformate

: N-(2-bromo-5-chlorophenyl)-4-methylbenzamide

: 40728-69-6
7-chloro-2-(p-tolyl)-4H-benzo[d][1,3]oxazin-4-one

Guidance literature:: With palladium diacetate; triethylamine; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In 1,4-dioxane; at 100 ℃; for 16h; Schlenk technique; Inert atmosphere;
DOI:10.1002/chem.202103137