3-[4-Acetyl-2,3,6-trihydroxy-5-(3-methyl-2-butenyl)benzyl]-6-ethyl-4-hydroxy-5-methyl-2H-pyran-2-one

Base Information

Chemical Name:3-[4-Acetyl-2,3,6-trihydroxy-5-(3-methyl-2-butenyl)benzyl]-6-ethyl-4-hydroxy-5-methyl-2H-pyran-2-one
CAS No.:32274-52-5
Molecular Formula:C₂₂H₂₆O₇
Molecular Weight:402.444
Hs Code.:
Mol file:32274-52-5.mol

Synonyms:2H-Pyran-2-one,3-[[3-acetyl-2,4,6-trihydroxy-5-(3-methyl-2-butenyl)phenyl]methyl]-6-ethyl-4-hydroxy-5-methyl-(9CI); Arzanol; Homoarenol

Suppliers and Price of 3-[4-Acetyl-2,3,6-trihydroxy-5-(3-methyl-2-butenyl)benzyl]-6-ethyl-4-hydroxy-5-methyl-2H-pyran-2-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Sigma-Aldrich
Arzanol from
1mg
$ 150.00

Adipogen Life Sciences
Arzanol ≥98%(NMR)
1 mg
$ 110.00

Total 1 raw suppliers

Chemical Property of 3-[4-Acetyl-2,3,6-trihydroxy-5-(3-methyl-2-butenyl)benzyl]-6-ethyl-4-hydroxy-5-methyl-2H-pyran-2-one

Chemical Property:

PSA：128.20000
LogP:3.63510
Storage Temp.:?20°C

Purity/Quality:

≥98% （HPLC） ^*data from raw suppliers

Arzanol from ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3-[4-Acetyl-2,3,6-trihydroxy-5-(3-methyl-2-butenyl)benzyl]-6-ethyl-4-hydroxy-5-methyl-2H-pyran-2-one

There total 4 articles about 3-[4-Acetyl-2,3,6-trihydroxy-5-(3-methyl-2-butenyl)benzyl]-6-ethyl-4-hydroxy-5-methyl-2H-pyran-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 31246-34-1
6-ethyl-4-hydroxy-5-methyl-α-pyrone

: 1030601-54-7
2,4-O-bis(tert-butyldimethylsilyl)-3-prenylphloracetophenone

: 33797-51-2
eschenmoser's salt

: 32274-52-5
arzanol

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; chloroform; at 40 ℃; for 16h;
DOI:10.1002/ejoc.201101193

Reference yield: 61.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 31246-34-1
6-ethyl-4-hydroxy-5-methyl-α-pyrone

: 1030601-54-7
2,4-O-bis(tert-butyldimethylsilyl)-3-prenylphloracetophenone

: 32274-52-5
arzanol

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; chloroform; at 40 ℃; for 16h;
DOI:10.1002/ejoc.201101193

Reference yield:

: 1372802-82-8
ethyl 4-methyl-3,5-dioxoheptanoate

: 32274-52-5
arzanol

Guidance literature:: Multi-step reaction with 2 steps

1: PPA / 1.5 h / 120 °C

2: tetrabutyl ammonium fluoride / tetrahydrofuran; chloroform / 16 h / 40 °C

With tetrabutyl ammonium fluoride; In tetrahydrofuran; PPA; chloroform;
DOI:10.1002/ejoc.201101193