1-Nonen-3-ol, 3-methyl-

Base Information

• Chemical Name: 1-Nonen-3-ol, 3-methyl-
• CAS No.: 22616-15-5
• Molecular Formula: C10H20 O
• Molecular Weight: 156.268
• Hs Code.: 2905290000
• DSSTox Substance ID: DTXSID90884896
• Nikkaji Number: J422.099D
• Mol file: 22616-15-5.mol

Synonyms:3-Methyl-1-nonen-3-ol;1-Nonen-3-ol, 3-methyl-;22616-15-5;AI3-24900;3-methylnon-1-en-3-ol;SCHEMBL4591909;DTXSID90884896;AKOS006272703

Chemical Property of 1-Nonen-3-ol, 3-methyl-

Chemical Property:

• Vapor Pressure: 0.094mmHg at 25°C
• Boiling Point: 197.9°Cat760mmHg
• Flash Point: 72.4°C
• PSA: 20.23000
• Density: 0.839g/cm³
• LogP: 2.89380
• XLogP3: 3.3
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 6
• Exact Mass: 156.151415257
• Heavy Atom Count: 11
• Complexity: 109

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCCCCCC(C)(C=C)O

Technology Process of 1-Nonen-3-ol, 3-methyl-

There total 7 articles about 1-Nonen-3-ol, 3-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

vinyl magnesium bromide (1826-67-1) + hexyl-methyl-ketone (111-13-7) → 3-methyl-non-1-en-3-ol (22616-15-5)

Guidance literature:

In tetrahydrofuran; at 0 - 20 ℃; Schlenk technique; Inert atmosphere;

DOI:10.1002/anie.202111648

Reference yield: 62.0%

methylenedimethyl sulfurane (6814-64-8,40651-06-7) + hexyl-methyl-ketone (111-13-7) → 3-methyl-non-1-en-3-ol (22616-15-5)

Guidance literature:

In tetrahydrofuran; 1.) -10 deg C to 0 deg C, 30 min, 2.) r.t., 2 h;

DOI:10.1016/S0040-4039(00)73035-8

Reference yield: 53.0%

(E)-3-Methyl-non-2-en-1-ol (72314-86-4) → 3-methyl-non-1-en-3-ol (22616-15-5)

Guidance literature:

bis(acetylacetonate)oxovanadium; bis-trimethylsilanyl peroxide; In dichloromethane; at 25 ℃; for 24h;

DOI:10.1016/S0040-4039(00)94523-4

upstream raw materials:

3-methyl-1-nonyn-3-ol

(E)-3-Methyl-non-2-en-1-ol

methylenedimethyl sulfurane

hexyl-methyl-ketone

Downstream raw materials:

3-nonanol, 3-methyl-

3-hexylthiophene

3-hexyl-2-bromothiophene