N,N'-(1,2-Di-4-pyridinyl-1,2-ethanediyl)bis-(1,1'-biphenyl)-4-carboxamide

Base Information

Chemical Name:N,N'-(1,2-Di-4-pyridinyl-1,2-ethanediyl)bis-(1,1'-biphenyl)-4-carboxamide
CAS No.:77502-39-7
Molecular Formula:C38H30 N4 O2
Molecular Weight:0
Hs Code.:2933399090
DSSTox Substance ID:DTXSID10998702
Mol file:77502-39-7.mol

Synonyms:77502-39-7;N,N'-(1,2-Di-4-pyridinyl-1,2-ethanediyl)bis-(1,1'-biphenyl)-4-carboxamide;(1,1'-Biphenyl)-4-carboxamide, N,N'-(1,2-di-4-pyridinyl-1,2-ethanediyl)bis-;DTXSID10998702;C38H30N4O2;C38-H30-N4-O2;LS-44231;N,N'-[1,2-Di(pyridin-4-yl)ethane-1,2-diyl]di([1,1'-biphenyl]-4-carboxamide)

Suppliers and Price of N,N'-(1,2-Di-4-pyridinyl-1,2-ethanediyl)bis-(1,1'-biphenyl)-4-carboxamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
N,N'-(1,2-DI-4-PYRIDINYL-1,2-ETHANEDIYL)BIS-(1,1'-BIPHENYL)-4-CARBOXAMIDE 95.00%
5MG
$ 499.05

Total 2 raw suppliers

Chemical Property of N,N'-(1,2-Di-4-pyridinyl-1,2-ethanediyl)bis-(1,1'-biphenyl)-4-carboxamide

Chemical Property:

Boiling Point:866.7oC at 760 mmHg
Flash Point:478oC
PSA：83.98000
Density:1.22g/cm3
LogP:8.23480
XLogP3:6.3
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:9
Exact Mass:574.23687621
Heavy Atom Count:44
Complexity:799

Purity/Quality:

99% ^*data from raw suppliers

N,N'-(1,2-DI-4-PYRIDINYL-1,2-ETHANEDIYL)BIS-(1,1'-BIPHENYL)-4-CARBOXAMIDE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)C2=CC=C(C=C2)C(=O)NC(C3=CC=NC=C3)C(C4=CC=NC=C4)NC(=O)C5=CC=C(C=C5)C6=CC=CC=C6

Technology Process of N,N'-(1,2-Di-4-pyridinyl-1,2-ethanediyl)bis-(1,1'-biphenyl)-4-carboxamide

There total 5 articles about N,N'-(1,2-Di-4-pyridinyl-1,2-ethanediyl)bis-(1,1'-biphenyl)-4-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 80819-03-0
Biphenyl-4-carboxylic acid (pyridin-4-ylmethyl)-amide

: 77502-55-7
Biphenyl-4-carboxylic acid (1-oxy-pyridin-4-ylmethyl)-amide

: 77502-39-7
C₃₈H₃₀N₄O₂

Guidance literature:: With acetic anhydride; at 70 ℃; for 3h;
DOI:10.1002/jhet.5570200658

Reference yield: 40.0%

: 77502-55-7
Biphenyl-4-carboxylic acid (1-oxy-pyridin-4-ylmethyl)-amide

: 77502-39-7
C₃₈H₃₀N₄O₂

Guidance literature:: In acetic anhydride; at 140 ℃; for 1.5h;
DOI:10.1002/jhet.5570180707

Reference yield:

: 3731-53-1
4-(aminomethyl)pyridine

: 77502-39-7
C₃₈H₃₀N₄O₂

Guidance literature:: Multi-step reaction with 3 steps

1: dicyclohexylcarbodiimide / acetonitrile / 24 h / Ambient temperature

2: 70 percent / hydrogen peroxide (40 percent) / acetic acid / 80 °C

3: 40 percent / acetic anhydride / 1.5 h / 140 °C

With dihydrogen peroxide; dicyclohexyl-carbodiimide; In acetic anhydride; acetic acid; acetonitrile;
DOI:10.1002/jhet.5570180707