9,10-Ethenoanthracene-11,12-dicarboxylic acid, 9,10-dihydro-

Base Information

• Chemical Name: 9,10-Ethenoanthracene-11,12-dicarboxylic acid, 9,10-dihydro-
• CAS No.: 1625-81-6
• Molecular Formula: C18H12 O4
• Molecular Weight: 292.291
• NSC Number: 22089
• UNII: ZNT3KX26DK
• DSSTox Substance ID: DTXSID90167378
• Nikkaji Number: J1.509.263G,J2.208.404F
• Wikidata: Q83036735
• Mol file: 1625-81-6.mol

Synonyms:9,10-Ethenoanthracene-11,12-dicarboxylic acid, 9,10-dihydro-;1625-81-6;9,10-dihydro-9,10-ethenoanthracene-11,12-dicarboxylic acid;NSC22089;ZNT3KX26DK;NSC-22089;NSC 22089;UNII-ZNT3KX26DK;SCHEMBL3186143;DTXSID90167378;RCL S244287;RCL S261602;AKOS024331418;9,10-dihydro-9,10-ethenoanthracene-11,12-dicar-boxylic acid;9,10-dihydro-9,10-ethenoanthracene-11,12-dicarboxylicacid;InChI=1/C18H12O4/c19-17(20)15-13-9-5-1-2-6-10(9)14(16(15)18(21)22)12-8-4-3-7-11(12)13/h1-8,13-14H,(H,19,20)(H,21,22

Chemical Property of 9,10-Ethenoanthracene-11,12-dicarboxylic acid, 9,10-dihydro-

Chemical Property:

• Vapor Pressure: 1.08E-11mmHg at 25°C
• Boiling Point: 521.3°Cat760mmHg
• Flash Point: 283.1°C
• Density: 1.488g/cm³
• XLogP3: 2.5
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 2
• Exact Mass: 292.07355886
• Heavy Atom Count: 22
• Complexity: 477

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C2C3C4=CC=CC=C4C(C2=C1)C(=C3C(=O)O)C(=O)O

Technology Process of 9,10-Ethenoanthracene-11,12-dicarboxylic acid, 9,10-dihydro-

There total 9 articles about 9,10-Ethenoanthracene-11,12-dicarboxylic acid, 9,10-dihydro- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

dimethyl 2,3,5,6-dibenzobicyclo-<2.2.2>octa-2,5,7-triene-7,8-dicarboxylate (1625-82-7) → 9,10-dihydro-9,10-diethylanthracene-11,12-dicarboxylic acid (1625-81-6)

Guidance literature:

With sodium hydroxide; In methanol; for 2h; Heating;

DOI:10.1002/hlca.19930760522

Reference yield: 99.0%

Dimethyl 9,10-dihydro-9,10-ethenoanthracene-11,12-dicarboxylate (1625-82-7) → 9,10-dihydro-9,10-ethenoanthracene-11,12-dicarboxylic acid (1625-81-6)

Guidance literature:

With potassium hydroxide; In ethanol; for 2h; Heating;

DOI:10.1016/S0040-4039(00)74241-9

Reference yield:

anthracene (120-12-7) → 9,10-dihydro-9,10-ethenoanthracene-11,12-dicarboxylic acid (1625-81-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 170 - 180 °C

2: NaOH; H₂O / methanol / 1 h / Heating

With sodium hydroxide; water; In methanol; 1: Diels-Alder reaction;

DOI:10.3390/50200179

upstream raw materials:

Dimethyl 9,10-dihydro-9,10-ethenoanthracene-11,12-dicarboxylate

anthracene

dimethyl 2,3,5,6-dibenzobicyclo-<2.2.2>octa-2,5,7-triene-7,8-dicarboxylate

tetrachloromethane

Downstream raw materials:

9,10-dihydro-9,10-etheno-11,12-anthracenedicarboxylic acid anhydride

9,10-dihydroanthracene-9,10-endo-α-acetoxy-α,β-succinic anhydride

N-phenyl-9,10-dihydro-9,10-ethenoanthracene-11,12-dicarboximide

N-(4-nitrophenyl)-9,10-dihydro-9,10-ethenoanthracene-11,12-dicarboximide