10-methylphenanthrene-9-carboxylic acid

Base Information

Chemical Name:10-methylphenanthrene-9-carboxylic acid
CAS No.:65698-59-1
Molecular Formula:C16H12O2
Molecular Weight:236.2653
Hs Code.:2916399090
Mol file:65698-59-1.mol

Synonyms:10-methyl-phenanthrene-9-carboxylic acid;10-Methyl-phenanthren-9-carbonsaeure;10-methyl-9-phenanthrenecarboxylic acid;

Suppliers and Price of 10-methylphenanthrene-9-carboxylic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 7 raw suppliers

Chemical Property of 10-methylphenanthrene-9-carboxylic acid

Chemical Property:

Vapor Pressure:1.4E-08mmHg at 25°C
Boiling Point:441.7°Cat760mmHg
Flash Point:199°C
PSA：37.30000
Density:1.267g/cm³
LogP:3.99960

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 10-methylphenanthrene-9-carboxylic acid

There total 5 articles about 10-methylphenanthrene-9-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 124-38-9,18923-20-1
carbon dioxide

: 52979-71-2
9-bromo-10-methyl-phenanthrene

: 65698-59-1
10-methylphenanthrene-9-carboxylic acid

Guidance literature:: With magnesium; Yield given. Multistep reaction; 1.) ether, reflux, 5 h, 2.) 4 h;
DOI:10.1021/jo00344a027

Reference yield:

: 52979-71-2
9-bromo-10-methyl-phenanthrene

: 65698-59-1
10-methylphenanthrene-9-carboxylic acid

Guidance literature:: With n-butyllithium; anschliessend Behandeln mit CO₂;

Reference yield:

: 883-20-5
9-methylphenanthrene

: 65698-59-1
10-methylphenanthrene-9-carboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: benzene; PBr₅

2: butyl lithium / anschliessend Behandeln mit CO₂

With n-butyllithium; phosphorus pentabromide; benzene;