Benzo(b)thiophen-3(2H)-one, 4-methoxy-7-(10-methoxy-5-methyl-4,5,6,7-tetrahydro-3H-furo(4,3,2-fg)(3)benzazocin-6-yl)-2-(phenylmethylene)-, 1,1-dioxide

Base Information

Chemical Name:Benzo(b)thiophen-3(2H)-one, 4-methoxy-7-(10-methoxy-5-methyl-4,5,6,7-tetrahydro-3H-furo(4,3,2-fg)(3)benzazocin-6-yl)-2-(phenylmethylene)-, 1,1-dioxide
CAS No.:155857-36-6
Molecular Formula:C₃₀H₂₇NO₆S
Molecular Weight:529.613
Hs Code.:

Benzo(b)thiophen-3(2H)-one, 4-methoxy-7-(10-methoxy-5-methyl-4,5,6,7-tetrahydro-3H-furo(4,3,2-fg)(3)benzazocin-6-yl)-2-(phenylmethylene)-, 1,1-dioxide

Synonyms:155857-36-6;Benzo(b)thiophen-3(2H)-one, 4-methoxy-7-(10-methoxy-5-methyl-4,5,6,7-tetrahydro-3H-furo(4,3,2-fg)(3)benzazocin-6-yl)-2-(phenylmethylene)-, 1,1-dioxide;C30H27NO6S;C30-H27-N-O6-S;LS-41317

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzo(b)thiophen-3(2H)-one, 4-methoxy-7-(10-methoxy-5-methyl-4,5,6,7-tetrahydro-3H-furo(4,3,2-fg)(3)benzazocin-6-yl)-2-(phenylmethylene)-, 1,1-dioxide

Chemical Property:

Vapor Pressure:3.76E-26mmHg at 25°C
Boiling Point:807.9°Cat760mmHg
Flash Point:442.4°C
Density:1.38g/cm³
XLogP3:2.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:7
Rotatable Bond Count:4
Exact Mass:529.15590875
Heavy Atom Count:38
Complexity:1250

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1CCC2C3=C1C(C=NC=C(C3=CO2)OC)C4=C5C(=C(C=C4)OC)C(=O)C(=CC6=CC=CC=C6)S5(=O)=O
Isomeric SMILES:CC1CCC2C3=C1C(C=N/C=C(\C3=CO2)/OC)C4=C5C(=C(C=C4)OC)C(=O)/C(=C/C6=CC=CC=C6)/S5(=O)=O

Technology Process of Benzo(b)thiophen-3(2H)-one, 4-methoxy-7-(10-methoxy-5-methyl-4,5,6,7-tetrahydro-3H-furo(4,3,2-fg)(3)benzazocin-6-yl)-2-(phenylmethylene)-, 1,1-dioxide

There total 4 articles about Benzo(b)thiophen-3(2H)-one, 4-methoxy-7-(10-methoxy-5-methyl-4,5,6,7-tetrahydro-3H-furo(4,3,2-fg)(3)benzazocin-6-yl)-2-(phenylmethylene)-, 1,1-dioxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 100-52-7
benzaldehyde

: 107672-79-7,155857-35-5
10-methoxy-6(4'-methoxy-benzo-2'-hydrothiophen-3'-on-S,S-dioxido)-5-methyl-3,4,6,7-tetrahydro-5H-furo(4.3.2-fg)-⁽³⁾-benzazacine

: 107672-83-3,155857-36-6
10-methoxy-6-<7'-(4'-methoxy-2'-benzylidenebenzothiophen-3'-one-1',1'-dioxido)>-5-methyl-3,4,6,7-tetrahydro-5H-furo<4,3,2-f,g><3>benzazocine

Guidance literature:: With ammonium chloride; acetic acid; for 8h; Heating;
DOI:10.1007/BF00780573

Reference yield:

: 107672-82-2
5-benzylidene-2-thiolen-4-one 1,1-dioxide

: 107672-83-3,155857-36-6
10-methoxy-6-<7'-(4'-methoxy-2'-benzylidenebenzothiophen-3'-one-1',1'-dioxido)>-5-methyl-3,4,6,7-tetrahydro-5H-furo<4,3,2-f,g><3>benzazocine

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / benzene / 3 h / Ambient temperature

2: 1) NaOMe; 2) NH₄Cl / aq. ethanol

With sodium methylate; ammonium chloride; In ethanol; benzene;
DOI:10.1016/S0040-4020(01)87458-5

Reference yield:

: 115-37-7
thebaine

: 107672-83-3,155857-36-6
10-methoxy-6-<7'-(4'-methoxy-2'-benzylidenebenzothiophen-3'-one-1',1'-dioxido)>-5-methyl-3,4,6,7-tetrahydro-5H-furo<4,3,2-f,g><3>benzazocine

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / benzene / 3 h / Ambient temperature

2: 1) NaOMe; 2) NH₄Cl / aq. ethanol

With sodium methylate; ammonium chloride; In ethanol; benzene;
DOI:10.1016/S0040-4020(01)87458-5