1-(2-Bromoethyl)-4-methylcyclohexane

Base Information

Chemical Name:1-(2-Bromoethyl)-4-methylcyclohexane
CAS No.:5452-69-7
Molecular Formula:C₉H₁₇Br
Molecular Weight:205.138
Hs Code.:
NSC Number:18971
DSSTox Substance ID:DTXSID30280878

Synonyms:1-(2-bromoethyl)-4-methylcyclohexane;5452-69-7;NSC18971;DTXSID30280878;NSC-18971;AKOS014104904;CS-0238170;EN300-1910050

Suppliers and Price of 1-(2-Bromoethyl)-4-methylcyclohexane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of 1-(2-Bromoethyl)-4-methylcyclohexane

Chemical Property:

Vapor Pressure:0.26mmHg at 25°C
Boiling Point:211.8°Cat760mmHg
Flash Point:79.4°C
Density:1.157g/cm³
XLogP3:4.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:2
Exact Mass:204.05136
Heavy Atom Count:10
Complexity:82.7

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1CCC(CC1)CCBr

Technology Process of 1-(2-Bromoethyl)-4-methylcyclohexane

There total 6 articles about 1-(2-Bromoethyl)-4-methylcyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4916-87-4
2-(4-methylcyclohexyl)ethanol

: 5452-69-7
1-(2-bromo-ethyl)-4-methyl-cyclohexane

Guidance literature:: With phosphorus tribromide;
DOI:10.1021/ja01873a004

Reference yield:

: 127180-76-1,42778-89-2,191113-70-9
ethyl 4-methylcyclohexylideneacetate

: 5452-69-7
1-(2-bromo-ethyl)-4-methyl-cyclohexane

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / H₂ / 5percent Pd/C / ethanol / 760 Torr

2: LiAlH₄ / tetrahydrofuran

3: PBr₃ / diethyl ether; diethyl ether / 16 h / Ambient temperature

With lithium aluminium tetrahydride; hydrogen; phosphorus tribromide; palladium on activated charcoal; In tetrahydrofuran; diethyl ether; ethanol;
DOI:10.1248/cpb.40.2391

Reference yield:

: 589-92-4
1-methylcyclohexan-4-one

: 5452-69-7
1-(2-bromo-ethyl)-4-methyl-cyclohexane

Guidance literature:: Multi-step reaction with 4 steps

1: 78 percent / NaH / benzene

2: 97 percent / H₂ / 5percent Pd/C / ethanol / 760 Torr

3: LiAlH₄ / tetrahydrofuran

4: PBr₃ / diethyl ether; diethyl ether / 16 h / Ambient temperature

With lithium aluminium tetrahydride; hydrogen; phosphorus tribromide; sodium hydride; palladium on activated charcoal; In tetrahydrofuran; diethyl ether; ethanol; benzene;
DOI:10.1248/cpb.40.2391