Tricyclohexyl borate

Base Information

Chemical Name:Tricyclohexyl borate
CAS No.:2467-16-5
Molecular Formula:C18H33 B O3
Molecular Weight:308.269
Hs Code.:2920909090
European Community (EC) Number:219-584-5
NSC Number:57115
DSSTox Substance ID:DTXSID8062442
Nikkaji Number:J216.109E
Wikidata:Q81990037
Mol file:2467-16-5.mol

Synonyms:Tricyclohexyl borate;2467-16-5;Boric acid, tricyclohexyl ester;Boric acid (H3BO3), tricyclohexyl ester;Tricyclohexyl orthoborate;Cyclohexyl borate;EINECS 219-584-5;AI3-60243;Tricyclohexyl borate #;Tris(cyclohexyloxy)borane;SCHEMBL51373;Boric acid tricyclohexyl ester;DTXSID8062442;C18H33BO3;Cyclohexyl borate, (C6H11O)3B;NSC57115;C18-H33-B-O3;NSC 57115;NSC-57115

Suppliers and Price of Tricyclohexyl borate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
TRICYCLOHEXYL BORATE 95.00%
5MG
$ 505.73

Total 7 raw suppliers

Chemical Property of Tricyclohexyl borate

Chemical Property:

Vapor Pressure:3.4E-05mmHg at 25°C
Melting Point:52-54 °C
Boiling Point:365°Cat760mmHg
Flash Point:123.5°C
PSA：27.69000
Density:0.99g/cm³
LogP:5.01920
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:6
Exact Mass:308.2522751
Heavy Atom Count:22
Complexity:247

Purity/Quality:

98%min ^*data from raw suppliers

TRICYCLOHEXYL BORATE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:B(OC1CCCCC1)(OC2CCCCC2)OC3CCCCC3

Technology Process of Tricyclohexyl borate

There total 8 articles about Tricyclohexyl borate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 11113-50-1,14635-83-7
boric acid

: 108-93-0
cyclohexanol

: 2467-16-5
tricyclohexyl borate

Guidance literature:: With calcium hydride; In neat (no solvent); byproducts: H2; react. under N2, slow addn. of the alcohol via syringe to B(OH)3 (ratio 3:1) and CaH2, cooling in a water bath, slow heating to 80-90°C for 12 h after abating the H2 gas evolution; distn. of the volatile products under reduced pressure (distn. pot temp. <= 120°C);

Reference yield: 50.0%

: U(BH₄)3(OC₆H₁₁)(C₄H₈O)2

: U(BH₄)2(OC₆H₁₁)2(C₄H₈O)2

: 2467-16-5
tricyclohexyl borate

Guidance literature:: With cyclohexanone; In tetrahydrofuran; addn. of cyclohexanone via microsyringe to U complex soln.; standing at room temp., 1h; reducing volume; addn. of pentane; cooling to -78°C; pptn.; rapid filtration, drying (vac.), elem. anal.; evapn. of mother liquor, extn. in pentane: B compd.;