9H-Carbazole, 3-[(2-chloro-4-nitrophenyl)azo]-

Base Information

• Chemical Name: 9H-Carbazole, 3-[(2-chloro-4-nitrophenyl)azo]-
• CAS No.: 64071-87-0
• Molecular Formula: C18H11 Cl N4 O2
• Molecular Weight: 350.764
• European Community (EC) Number: 264-657-7
• DSSTox Substance ID: DTXSID3070044
• Nikkaji Number: J310.041C
• Mol file: 64071-87-0.mol

Synonyms:64071-87-0;EINECS 264-657-7;3-((2-Chloro-4-nitrophenyl)azo)carbazole;9H-Carbazole, 3-[(2-chloro-4-nitrophenyl)azo]-;3-[(2-Chloro-4-nitrophenyl)azo]-9H-carbazole;9H-Carbazole, 3-((2-chloro-4-nitrophenyl)azo)-;C18H11ClN4O2;9H-Carbazole, 3-(2-(2-chloro-4-nitrophenyl)diazenyl)-;3-((2-Chloro-4-nitrophenyl)azo)-9H-carbazole;DTXSID3070044;C18-H11-Cl-N4-O2;3-(2-Chloro-4-nitrophenylazo)-9H-carbazole

Chemical Property of 9H-Carbazole, 3-[(2-chloro-4-nitrophenyl)azo]-

Chemical Property:

• Vapor Pressure: 3.53E-14mmHg at 25°C
• Boiling Point: 610.2°C at 760 mmHg
• Flash Point: 322.8°C
• PSA: 86.33000
• Density: 1.47g/cm³
• LogP: 6.82130
• XLogP3: 5.6
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 2
• Exact Mass: 350.0570533
• Heavy Atom Count: 25
• Complexity: 526

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C2C(=C1)C3=C(N2)C=CC(=C3)N=NC4=C(C=C(C=C4)[N+](=O)[O-])Cl

Technology Process of 9H-Carbazole, 3-[(2-chloro-4-nitrophenyl)azo]-

There total 1 articles about 9H-Carbazole, 3-[(2-chloro-4-nitrophenyl)azo]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

9H-carbazole (86-74-8,105184-46-1,97960-57-1) + 2-Chloro-4-nitroaniline (121-87-9) → 3-(2'-chloro-4'-nitrophenylazo)carbazole (64071-87-0)

Guidance literature:

2-Chloro-4-nitroaniline; With hydrogenchloride; sodium nitrite; In water; for 0.5h; Cooling with ice;

9H-carbazole; In water; butan-1-ol; at 40 ℃;

DOI:10.1080/15421400801926396

Reference yield: 70.0%

3-(2'-chloro-4'-nitrophenylazo)carbazole (64071-87-0) + epichlorohydrin (106-89-8,24969-06-0,13403-37-7) → 3-(2'-chloro-4'-nitrophenylazo)-N-(2,3-epoxyprpyl)-carbazole (792931-67-0)

Guidance literature:

With potassium hydroxide; tetrabutylammomium bromide; potassium carbonate; In acetone; at 35 ℃; for 6h;

DOI:10.1080/15421400801926396

upstream raw materials:

9H-carbazole

2-Chloro-4-nitroaniline

Downstream raw materials:

3-(2'-chloro-4'-nitrophenylazo)-N-(2,3-epoxyprpyl)-carbazole

Refernces