2-({N-[(benzyloxy)carbonyl]glycyl}amino)prop-2-enoic acid

Base Information

Chemical Name:2-({N-[(benzyloxy)carbonyl]glycyl}amino)prop-2-enoic acid
CAS No.:62076-55-5
Molecular Formula:C13H14N2O5
Molecular Weight:278.265
Hs Code.:
NSC Number:179193
DSSTox Substance ID:DTXSID60306671
Nikkaji Number:J1.172.286E
Wikidata:Q82053868

Synonyms:62076-55-5;NSC179193;DTXSID60306671;NSC-179193;2-({N-[(benzyloxy)carbonyl]glycyl}amino)prop-2-enoic acid

Suppliers and Price of 2-({N-[(benzyloxy)carbonyl]glycyl}amino)prop-2-enoic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 7 raw suppliers

Chemical Property of 2-({N-[(benzyloxy)carbonyl]glycyl}amino)prop-2-enoic acid

Chemical Property:

Vapor Pressure:1.48E-15mmHg at 25°C
Refractive Index:1.563
Boiling Point:606.4 °C at 760 mmHg
Flash Point:320.5 °C
Density:1.309 g/cm³
XLogP3:1
Hydrogen Bond Donor Count:3
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:7
Exact Mass:278.09027155
Heavy Atom Count:20
Complexity:388

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C=C(C(=O)O)NC(=O)CNC(=O)OCC1=CC=CC=C1

Technology Process of 2-({N-[(benzyloxy)carbonyl]glycyl}amino)prop-2-enoic acid

There total 4 articles about 2-({N-[(benzyloxy)carbonyl]glycyl}amino)prop-2-enoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 949-90-6
N-(carbobenzyloxy)glycinamide

: 127-17-3
2-oxo-propionic acid

: 62076-55-5
Z-Gly-ΔAla

Guidance literature:: With toluene-4-sulfonic acid; In benzene; for 6h; Heating;

Reference yield:

: 10367-06-3
Gly-ΔAla

: 501-53-1,94274-21-2
benzyl chloroformate

: 62076-55-5
Z-Gly-ΔAla

Guidance literature:: With sodium hydroxide;
DOI:10.1021/ja01060a049

Reference yield:

: 1138-80-3
N-(Benzyloxycarbonyl)glycine

: 62076-55-5
Z-Gly-ΔAla

Guidance literature:: Multi-step reaction with 2 steps

1: (i) Et₃N, AcOEt, (ii) ClCO₂sBu, (iii) /BRN= 5112410/

2: (i) HCO₂H, (ii) aq. NaOH

DOI:10.1021/ja01060a050