5-Bromo-1,2,3,4-tetrahydronaphthalene

Base Information

• Chemical Name: 5-Bromo-1,2,3,4-tetrahydronaphthalene
• CAS No.: 6134-55-0
• Molecular Formula: C10H11 Br
• Molecular Weight: 211.101
• Hs Code.: 2903999090
• NSC Number: 174089
• UNII: 69SPU3D3DM
• DSSTox Substance ID: DTXSID40210247
• Nikkaji Number: J460.839I
• Wikidata: Q83084874
• Mol file: 6134-55-0.mol

Synonyms:5-Bromo-1,2,3,4-tetrahydronaphthalene;6134-55-0;5-Bromo-1,2,3,4-tetrahydro-naphthalene;Naphthalene, 5-bromo-1,2,3,4-tetrahydro-;69SPU3D3DM;NSC-174089;NSC174089;NSC 174089;1-bromo-5,6,7,8-tetrahydronaphthalene;EC-000.1738;UNII-69SPU3D3DM;SCHEMBL1513618;DTXSID40210247;WDNLCUAIHSXPBR-UHFFFAOYSA-N;MFCD08361743;AKOS015835484;MB06103;AC-31672;BS-29124;CS-0159081;FT-0685618;5-Bromo-1,2,3,4-tetrahydro-naphthalene 97%;N12384;A868734;J-516773;5-bromo-1,2,3,4-tetrahydro-naphthalene, AldrichCPR

Chemical Property of 5-Bromo-1,2,3,4-tetrahydronaphthalene

Chemical Property:

• Vapor Pressure: 0.0107mmHg at 25°C
• Boiling Point: 271.4°C at 760 mmHg
• Flash Point: 119.6°C
• PSA: 0.00000
• Density: 1.384g/cm³
• LogP: 3.32790
• Storage Temp.: Sealed in dry,Room Temperature
• XLogP3: 4
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 0
• Exact Mass: 210.00441
• Heavy Atom Count: 11
• Complexity: 133

Purity/Quality:

98% ^*data from raw suppliers

5-Bromo-1,2,3,4-tetrahydronaphthalene ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xn,N
• Statements: 22-51/53
• Safety Statements: 61

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1CCC2=C(C1)C=CC=C2Br

Technology Process of 5-Bromo-1,2,3,4-tetrahydronaphthalene

There total 18 articles about 5-Bromo-1,2,3,4-tetrahydronaphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

tetralin (119-64-2) → 5-bromotetralin (6134-55-0)

Guidance literature:

With aluminum oxide; bromine; for 0.0166667h; Ambient temperature;

DOI:10.1080/00397919208021092

Reference yield: 90.0%

trans-6,7-Dibromo-11-oxatricyclo<5.3.1.01,6>undecane → 5-bromotetralin (6134-55-0)

Guidance literature:

for 84h;

DOI:10.1021/jo00114a018

Reference yield: 51.0%

1,2-diethynylcyclohex-1-ene (21336-06-1) → 5-bromotetralin (6134-55-0)

Guidance literature:

With hydrogen bromide; In water; at 100 ℃; for 8h;

DOI:10.1021/jo0518295

upstream raw materials:

1-amino-5,6,7,8-tetrahydronaphthalene

tetralin

Cyclodeca-1,3-dien-5-yn-1-yl trifluoromethanesulphonate

1,2-diethynylcyclohex-1-ene

Downstream raw materials:

ethyl 5-(4-chlorophenyl)-4-methyl-3-(4-sulfamoyl-5,6,7,8-tetrahydronaphthalen-1-yl)thiophene-2-carboxylate

4-[5,6,7,8-tetrahydronaphthalen-1-yl]phenol

5,6,7,8-tetrahydro-1-naphthalenecarboxylic acid

1,2,3,4-tetrahydro-2-naphthoic acid

Refernces

• 1、 Fieser,Seligman. "-". . p. 478. Retrieved 1936.
• 2、 Nishii, Yuji,Ikeda, Mitsuhiro,Hayashi, Yoshihiro,Kawauchi, Susumu,Miura, Masahiro. "Triptycenyl Sulfide: A Practical and Active Catalyst for Electrophilic Aromatic Halogenation Using N-Halosuccinimides". supporting information. p. 1621 - 1629. Retrieved 2020/02/04.
• 3、 -. "GLYCOLATE OXIDASE INHIBITORS FOR THE TREATMENT OF DISEASE". Paragraph 001329; 001330; 001331. . Retrieved 2019/07/17.