N,N-Diethyl-alpha,beta-dimethyl-trans-cinnamamide

Base Information

Chemical Name:N,N-Diethyl-alpha,beta-dimethyl-trans-cinnamamide
CAS No.:5422-03-7
Molecular Formula:C15H21 N O
Molecular Weight:231.3333
Hs Code.:
NSC Number:8355
DSSTox Substance ID:DTXSID10420937
Nikkaji Number:J1.656.863E
Wikidata:Q82232257

Synonyms:NSC8355;5422-03-7;DTXSID10420937;NSC-8355;N,N-Diethyl-alpha,beta-dimethyl-trans-cinnamamide

Suppliers and Price of N,N-Diethyl-alpha,beta-dimethyl-trans-cinnamamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of N,N-Diethyl-alpha,beta-dimethyl-trans-cinnamamide

Chemical Property:

Vapor Pressure:1.62E-05mmHg at 25°C
Boiling Point:365°Cat760mmHg
Flash Point:160.8°C
Density:0.976g/cm³
XLogP3:3.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:4
Exact Mass:231.162314293
Heavy Atom Count:17
Complexity:283

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCN(CC)C(=O)C(=C(C)C1=CC=CC=C1)C
Isomeric SMILES:CCN(CC)C(=O)/C(=C(\C)/C1=CC=CC=C1)/C

Technology Process of N,N-Diethyl-alpha,beta-dimethyl-trans-cinnamamide

There total 6 articles about N,N-Diethyl-alpha,beta-dimethyl-trans-cinnamamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 600734-14-3
2,3-epoxy-N,N-diethyl-2-methyl-3-phenylbutanamide

: 5422-03-7
(E)-N,N-diethyl-2-methyl-3-phenylbut-2-enamide

Guidance literature:: With samarium diiodide; In tetrahydrofuran; at 25 ℃; for 0.5h;
DOI:10.1021/jo0349577

Reference yield:

: 2-Chloro-N,N-diethyl-3-hydroxy-2-methyl-3-phenylbutanamide

: 5422-03-7
(E)-N,N-diethyl-2-methyl-3-phenylbut-2-enamide

: (Z)-N,N-Diethyl-2-methyl-3-phenylbut-2-enamide

Guidance literature:: With samarium diiodide; In tetrahydrofuran; at -25 ℃; for 2.5h; Title compound not separated from byproducts.;
DOI:10.1002/1521-3765(20010716)7:14<3062::AID-CHEM3062>3.0.CO;2-F

Reference yield:

: 54333-75-4
2-chloro-N,N-diethylpropionamide

: 5422-03-7
(E)-N,N-diethyl-2-methyl-3-phenylbut-2-enamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: lithium diisopropylamide / tetrahydrofuran / 0.17 h / -78 °C

1.2: 90 percent / tetrahydrofuran / -78 - 25 °C

2.1: 95 percent / SmI₂ / tetrahydrofuran / 0.5 h / 25 °C

With samarium diiodide; lithium diisopropyl amide; In tetrahydrofuran;
DOI:10.1021/jo0349577