TRANS-DIBENZ(A,J)ACRIDINE-5,6-DIHYDRODIOL

Base Information

Chemical Name:TRANS-DIBENZ(A,J)ACRIDINE-5,6-DIHYDRODIOL
CAS No.:105467-64-9
Molecular Formula:C₂₁H₁₅NO₂
Molecular Weight:313.356
Hs Code.:
Mol file:105467-64-9.mol

Synonyms:trans-5,6-Dihydro-5,6-dihydroxydibenz[a,j]acridine;trans-5,6-Dihydrodibenz[a,j]acridine-5,6-diol; trans-Dibenz[a,j]acridine-5,6-dihydrodiol

Suppliers and Price of TRANS-DIBENZ(A,J)ACRIDINE-5,6-DIHYDRODIOL

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of TRANS-DIBENZ(A,J)ACRIDINE-5,6-DIHYDRODIOL

Chemical Property:

Vapor Pressure:6.16E-15mmHg at 25°C
Boiling Point:593.6°Cat760mmHg
Flash Point:312.8°C
PSA：53.35000
Density:1.414g/cm³
LogP:4.13540

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of TRANS-DIBENZ(A,J)ACRIDINE-5,6-DIHYDRODIOL

There total 13 articles about TRANS-DIBENZ(A,J)ACRIDINE-5,6-DIHYDRODIOL which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 106589-66-6
dibenzacridine-5,6-quinone

: 105467-64-9,106589-64-4,117019-82-6,117019-83-7,117019-84-8,117019-85-9,117066-35-0
trans-5,6-dihydro-5,6-dihydroxydibenzacridine

Guidance literature:: With sodium tetrahydroborate; In methanol; for 3h;
DOI:10.1021/jo00382a017

Reference yield:

: 5419-02-3
1-dimethylaminomethyl-naphthalen-2-ol

: 105467-64-9,106589-64-4,117019-82-6,117019-83-7,117019-84-8,117019-85-9,117066-35-0
trans-5,6-dihydro-5,6-dihydroxydibenzacridine

Guidance literature:: Multi-step reaction with 6 steps

1: 0.5 g / 0.5 h / 260 - 280 °C

2: 83 percent / 10percent Pd/C / various solvent(s) / 8 h / 190 °C

3: 9 percent / NH₄HSO₄, 5percent aq. NaClO / CH₂Cl₂ / 6 h

4: 78 percent / 25percent CH₃COOH / dioxane / 36 h / Ambient temperature

5: 72 percent / benzeneselenic anhydride / tetrahydrofuran / 5 h / 50 °C

6: 81 percent / NaBH₄ / methanol / 3 h

With ammonium bisulphate; sodium hypochlorite; sodium tetrahydroborate; benzeneseleninic anhydride; acetic acid; palladium on activated charcoal; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane;
DOI:10.1021/jo00382a017

Reference yield:

: 2217-43-8
6-amino-1,2,3,4-tetrahydronaphthalene

: 105467-64-9,106589-64-4,117019-82-6,117019-83-7,117019-84-8,117019-85-9,117066-35-0
trans-5,6-dihydro-5,6-dihydroxydibenzacridine

Guidance literature:: Multi-step reaction with 6 steps

1: 0.5 g / 0.5 h / 260 - 280 °C

2: 83 percent / 10percent Pd/C / various solvent(s) / 8 h / 190 °C

3: 9 percent / NH₄HSO₄, 5percent aq. NaClO / CH₂Cl₂ / 6 h

4: 78 percent / 25percent CH₃COOH / dioxane / 36 h / Ambient temperature

5: 72 percent / benzeneselenic anhydride / tetrahydrofuran / 5 h / 50 °C

6: 81 percent / NaBH₄ / methanol / 3 h

With ammonium bisulphate; sodium hypochlorite; sodium tetrahydroborate; benzeneseleninic anhydride; acetic acid; palladium on activated charcoal; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane;
DOI:10.1021/jo00382a017