(1-benzylpyridin-4(1H)-ylidene)-N-oxomethanaminium chloride

Base Information

• Chemical Name: (1-benzylpyridin-4(1H)-ylidene)-N-oxomethanaminium chloride
• CAS No.: 7375-29-3
• Molecular Formula: C₁₃H₁₃N₂O*Cl
• Molecular Weight: 248.712
• Mol file: 7375-29-3.mol

Synonyms:

Chemical Property of (1-benzylpyridin-4(1H)-ylidene)-N-oxomethanaminium chloride

Chemical Property:

• Vapor Pressure: 0.00017mmHg at 25°C
• Boiling Point: 330.1°Cat760mmHg
• Flash Point: 153.4°C
• Density: g/cm³

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (1-benzylpyridin-4(1H)-ylidene)-N-oxomethanaminium chloride

There total 1 articles about (1-benzylpyridin-4(1H)-ylidene)-N-oxomethanaminium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.4%

4-pyridinealdoxime (1637-52-1) + benzyl chloride (100-44-7) → 1-benzylpyridinium-4-aldoxime chloride (7375-29-3)

Guidance literature:

In ethanol; at 20 ℃; for 168h;

DOI:10.1016/j.ica.2010.01.041

Reference yield: 26.1%

sodium amminepentacyanoferrate(II) trihydrate + water (7732-18-5) + 1-benzylpyridinium-4-aldoxime chloride (7375-29-3) → [1-benzylpyridinium-4-aldoxime]2[Fe(CN)5(1-benzylpyridinium-4-aldoxime)]*3H2O

Guidance literature:

In water; Aq. soln. of ligand added to aq. soln. of Fe compd. (5:1 molar ratio), pH about 6; ppt. filtered off, washed (water), dried (vac., over P2O5), elem. anal.;

DOI:10.1016/j.ica.2010.01.041

Reference yield:

trisodium aquapentacyanoferrate + 1-benzylpyridinium-4-aldoxime chloride (7375-29-3) → [Fe(CN)5(N-benzylpyridinium-4-aldoxime)]-2

Guidance literature:

In water; in buffered soln. (pH 8, Britton-Robinson buffer) at 16 to 28°C, ionic strength maintained constant with NaCl, oxime ligand always present in excess; not isolated, react. monitored by absorption spect.; Kinetics;

upstream raw materials:

4-pyridinealdoxime

benzyl chloride