2-methyl-3,4-dihydro-1H-isoquinoline-4,6,7-triol

Base Information

Chemical Name:2-methyl-3,4-dihydro-1H-isoquinoline-4,6,7-triol
CAS No.:82563-75-5
Molecular Formula:C₁₀H₁₃NO₃
Molecular Weight:195.218
Hs Code.:
Mol file:82563-75-5.mol

Synonyms:4,6,7-Isoquinolinetriol,1,2,3,4-tetrahydro-2-methyl;TMIQ;1,2,3,4-tetrahydro-4,6,7-trihydroxy-2-methylisoquinoline;

Suppliers and Price of 2-methyl-3,4-dihydro-1H-isoquinoline-4,6,7-triol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 2-methyl-3,4-dihydro-1H-isoquinoline-4,6,7-triol

Chemical Property:

Vapor Pressure:2.91E-07mmHg at 25°C
Boiling Point:404.3°Cat760mmHg
Flash Point:244.7°C
PSA：63.93000
Density:1.382g/cm³
LogP:0.51450

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-methyl-3,4-dihydro-1H-isoquinoline-4,6,7-triol

There total 3 articles about 2-methyl-3,4-dihydro-1H-isoquinoline-4,6,7-triol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 23.7%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 329-65-7,51028-73-0
Epinephrine

: 72812-48-7,82563-75-5
1,2,3,4-tetrahydro-4,6,7-trihydroxy-2-methylisoquinoline

Guidance literature:: In methanol; for 1h; Ambient temperature;
DOI:10.1248/cpb.30.1352

Reference yield: 8.1%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 329-65-7,51028-73-0
Epinephrine

: 82334-24-5
1,2,3,4-tetrahydro-4,7,8-trihydroxy-2-methylisoquinoline

: 72812-48-7,82563-75-5
1,2,3,4-tetrahydro-4,6,7-trihydroxy-2-methylisoquinoline

Guidance literature:: With hydrogenchloride; ascorbic acid; In water; for 1h; Ambient temperature; in Tris-HCl buffer, pH 7.0;
DOI:10.1248/cpb.30.1352

Reference yield:

: 51-42-3,636-89-5,1234-55-5,2964-12-7,14479-84-6,19947-47-8,21282-30-4,24351-82-4,40004-76-0,55750-10-2,69207-54-1,104655-01-8,16536-89-3,8028-06-6
(-)-Noradrenaline bitartrate

: 50-81-7,98966-42-8
ascorbic acid

: 82334-24-5
1,2,3,4-tetrahydro-4,7,8-trihydroxy-2-methylisoquinoline

: 72812-48-7,82563-75-5
1,2,3,4-tetrahydro-4,6,7-trihydroxy-2-methylisoquinoline

Guidance literature:: With oxygen; In water; at 60 ℃; for 3h; Yield given. Yields of byproduct given; 0.1 M phosphate buffer, pH 7.0;
DOI:10.1248/cpb.30.1352