2,6-Octadiyne

Base Information

Chemical Name:2,6-Octadiyne
CAS No.:764-73-8
Molecular Formula:C8H10
Molecular Weight:106.167
Hs Code.:
Mol file:764-73-8.mol

Synonyms:2,6-OCTADIYNE;octa-2,6-diyne

Suppliers and Price of 2,6-Octadiyne

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
2,6-Octadiyne
2mg
$ 60.00

TCI Chemical
2,6-Octadiyne >97.0%(GC)
0.1mL
$ 106.00

AK Scientific
2,6-Octadiyne
100uL
$ 217.00

Total 10 raw suppliers

Chemical Property of 2,6-Octadiyne

Chemical Property:

Vapor Pressure:4.11mmHg at 25°C
Melting Point:27°C
Refractive Index:1.4658
Boiling Point:62°C 19mm
Flash Point:27 °C
PSA：0.00000
Density:0,828 g/cm3
LogP:1.81320

Purity/Quality:

98%,99%, ^*data from raw suppliers

2,6-Octadiyne ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:
Statements: 10
Safety Statements: 16

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2,6-Octadiyne

There total 2 articles about 2,6-Octadiyne which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 503-17-3
dimethylacetylene

: 764-73-8
octa-2,6-diyne

: 87-85-4
Hexamethylbenzene

: 33719-64-1
3-methyl-hept-2-en-5-yne

: 20380-32-9
octamethyl-(1rH,2cH,5cH,6cH)-tricyclo[4.2.0.0^2,5]octa-3,7-diene

Guidance literature:: for 160h; Further byproducts given; Irradiation;
DOI:10.1021/ja00742a019

Reference yield:

: 3355-28-0
1-Bromo-2-butyne

: 764-35-2
2-Hexyne

: 764-73-8
octa-2,6-diyne

Guidance literature:: With diethyl ether; ethylmagnesium bromide;

Reference yield: 96.0%

: 82581-56-4
NEt₄{Nb(CO)6}

: 764-73-8
octa-2,6-diyne

: 7553-56-2,12190-71-5,8031-47-8
iodine

: 554-70-1
triethylphosphine

: 168559-03-3
all-trans-[INb(CO)2(PMe₂Ph)2(2,8-octadiyne)]

Guidance literature:: In tetrahydrofuran; byproducts: Et4NI, CO; inert atmosphere; addn. of phoshine to Nb-complex, cooling in dry ice, addn. of I2, slow warming to room temp. overnight, filtration, addn. of alkyne, stirring; solvent removal (vac.), washing (hexane), dissoln. in CH2Cl2, evapn., drying (vac.);
DOI:10.1016/0022-328X(95)05493-9