Periplocoside N

Base Information

• Chemical Name: Periplocoside N
• CAS No.: 39946-41-3
• Molecular Formula: C27H44O6
• Molecular Weight: 464.63
• Mol file: 39946-41-3.mol

Synonyms:5-pregnene-3,17,20(S)-triol 20-O--D-canaropyranoside (periplocoside N);periplocoside N;(2R,3S,4R,6S)-6-[(S)-1-((3S,8R,9S,10R,13S,14S,17R)-3,17-Dihydroxy-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-17-yl)-ethoxy]-2-methyl-tetrahydro-pyran-3,4-diol;Δ5-pregnene-3β,17α,20(S)-triol 20-O-β-D-canaropyranoside;

Chemical Property of Periplocoside N

Chemical Property:

• PSA: 99.38000
• LogP: 3.30300

Purity/Quality:

HPLC≥98% ^*data from raw suppliers

Periplocoside N ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Periplocoside N

There total 2 articles about Periplocoside N which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

periploside A (110782-04-2) → (3S,8R,9S,10R,13S,14S,17R)-17-[(S)-1-((2S,4R,5R,6R)-5-Hydroxy-4-methoxymethoxy-6-methyl-tetrahydro-pyran-2-yloxy)-ethyl]-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthrene-3,17-diol (110764-08-4) + 2-O-acetyl-β-D-digitalopyranosyl(1->4)-β-D-cymaropyranosyl(1->4)-β-D-cymaropyranosyl(1->4)-β-D-cymaropyranosyl(1->4)-β-D-oleandronic-δ-lactone (110764-09-5) + Δ5-pregnene-3β,17α,20(S)-triol 20-O-β-D-canaropyranoside (periplocoside N) (39946-41-3)

Guidance literature:

With sulfuric acid; In methanol;

Reference yield:

Δ5-pregnene 3β,17α,20(S)-triol 20-O-β-D-digitalopyranosyl-(1->4)-β-D-cymaropyranosyl-(1->4)-β-D-canoropyranosyl-(1->4)-β-D-digitoxopyranosyl-(1->5)-3,7-dideoxy-4-O-methyl-α-D-gluco-2-heptulopyranosyl-(2-4)-dideoxy-(1->3)-β-D-canaropyranoside (119902-15-7) → Δ5-pregnene-3β,17α,20α-triol (903-67-3) + β-D-digitalopyranosyl-(1->4)-β-D-cymaropyranosyl-(1->4)-β-D-canaropyranosyl-(1->4)-β-D-digitoxopyranosyl-(1->4)-D-oleandro-1,5-lactone (119902-18-0) + Δ5-pregnene-3β,17α,20(S)-triol 20-O-β-D-canaropyranoside (periplocoside N) (39946-41-3)

Guidance literature:

With sulfuric acid; In methanol; for 0.5h; Further byproducts given; Ambient temperature;

DOI:10.1248/cpb.36.4441

Reference yield:

Δ5-pregnene-3β,17α,20(S)-triol 20-O-β-D-canaropyranoside (periplocoside N) (39946-41-3) → Δ5-pregnene-3β,17α,20α-triol (903-67-3)

Guidance literature:

With sulfuric acid; In methanol; Heating;

upstream raw materials:

Δ⁵-pregnene 3β,17α,20(S)-triol 20-O-β-D-digitalopyranosyl-(1->4)-β-D-cymaropyranosyl-(1->4)-β-D-canoropyranosyl-(1->4)-β-D-digitoxopyranosyl-(1->5)-3,7-dideoxy-4-O-methyl-α-D-gluco-2-heptulopyranosyl-(2-4)-dideoxy-(1->3)-β-D-canaropyranoside

periploside A

Downstream raw materials:

Δ⁵-pregnene-3β,17α,20α-triol

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