2'-(p-Tosyl)(3,4,5-trimethoxybenzo)hydrazide

Base Information

• Chemical Name: 2'-(p-Tosyl)(3,4,5-trimethoxybenzo)hydrazide
• CAS No.: 13513-93-4
• Molecular Formula: C17H20 N2 O6 S
• Molecular Weight: 380.422
• Hs Code.: 2935009090
• European Community (EC) Number: 236-851-1
• NSC Number: 92966
• DSSTox Substance ID: DTXSID20159261
• Nikkaji Number: J241.163F
• Mol file: 13513-93-4.mol

Synonyms:2'-(p-Tosyl)(3,4,5-trimethoxybenzo)hydrazide;13513-93-4;EINECS 236-851-1;NSC92966;3,4,5-trimethoxy-n'-[(4-methylphenyl)sulfonyl]benzohydrazide;DTXSID20159261;NSC 92966;NSC-92966;AKOS003413015

Chemical Property of 2'-(p-Tosyl)(3,4,5-trimethoxybenzo)hydrazide

Chemical Property:

• Boiling Point: °Cat760mmHg
• Flash Point: °C
• PSA: 111.34000
• Density: 1.282g/cm³
• LogP: 3.50670
• XLogP3: 2.3
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 7
• Rotatable Bond Count: 7
• Exact Mass: 380.10420754
• Heavy Atom Count: 26
• Complexity: 542

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=CC=C(C=C1)S(=O)(=O)NNC(=O)C2=CC(=C(C(=C2)OC)OC)OC

Technology Process of 2'-(p-Tosyl)(3,4,5-trimethoxybenzo)hydrazide

There total 3 articles about 2'-(p-Tosyl)(3,4,5-trimethoxybenzo)hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ethyl 3,4,5-trimethoxybenzoate (6178-44-5) → N-(tolul-4-sulfonyl)-N'-(3,4,5-trimethoxy-benzoyl)-hydrazine (13513-93-4)

Guidance literature:

Multi-step reaction with 2 steps

1: diethyl ether; aqueous hydrazine hydrate

2: pyridine

With pyridine; diethyl ether; hydrazine hydrate;

Reference yield:

3,4,5-trimethoxybenzohydrazide (3291-03-0) + p-toluenesulfonyl chloride (98-59-9) → N-(tolul-4-sulfonyl)-N'-(3,4,5-trimethoxy-benzoyl)-hydrazine (13513-93-4)

Guidance literature:

With pyridine;

Reference yield:

→ N-(tolul-4-sulfonyl)-N'-(3,4,5-trimethoxy-benzoyl)-hydrazine (13513-93-4)

Guidance literature:

3.4.5-Trimethoxy-benzoesaeurehydrazid (VI), Py., Tosylchlorid, Δ;

upstream raw materials:

3,4,5-trimethoxybenzohydrazide

p-toluenesulfonyl chloride

ethyl 3,4,5-trimethoxybenzoate