4-((3,4-Dimethylbenzoyl)amino)-5-oxopentanoic acid

Base Information

Chemical Name:4-((3,4-Dimethylbenzoyl)amino)-5-oxopentanoic acid
CAS No.:97964-53-9
Molecular Formula:C22H34N2O4
Molecular Weight:390.5164
Hs Code.:
DSSTox Substance ID:DTXSID80913523

Synonyms:4-((3,4-dimethylbenzoyl)amino)-5-oxopentanoic acid;CR 1372;CR-1372

Suppliers and Price of 4-((3,4-Dimethylbenzoyl)amino)-5-oxopentanoic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 1 raw suppliers

Chemical Property of 4-((3,4-Dimethylbenzoyl)amino)-5-oxopentanoic acid

Chemical Property:

Vapor Pressure:1.46E-14mmHg at 25°C
Boiling Point:585.7°Cat760mmHg
Flash Point:308°C
PSA：86.71000
Density:1.085g/cm³
LogP:4.08630
XLogP3:3.8
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:12
Exact Mass:390.25185757
Heavy Atom Count:28
Complexity:501

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CCCCN(CCCC)C(=O)C(CCC(=O)O)NC(=O)C1=CC(=C(C=C1)C)C

Technology Process of 4-((3,4-Dimethylbenzoyl)amino)-5-oxopentanoic acid

There total 8 articles about 4-((3,4-Dimethylbenzoyl)amino)-5-oxopentanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 111-92-2
dibutylamine

: 102743-18-0
3,4-dimethyl-N-benzoyl-DL-glutamic anhydride

: 97964-53-9
(+/-)-CR 1372

: 102768-06-9
DL-2-(3,4-dimethyl-benzoyl-amino)-5-(di-n-butyl-amino)-5-oxo-pentanoic acid

Guidance literature:: In water; at 5 - 10 ℃; for 3h;

Reference yield:

: 21900-23-2
3,4-dimethylbenzoyl chloride

: 97964-53-9
(+/-)-CR 1372

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / 1N NaOH / H₂O / 4 h / 15 - 20 °C

2: 82.5 percent / acetic anhydride / diisopropyl ether / 2 h / 70 °C

3: tetrahydrofuran / 3 h / 25 °C

With sodium hydroxide; acetic anhydride; In tetrahydrofuran; di-isopropyl ether; water;