Tridecan-7-one oxime

Base Information

• Chemical Name: Tridecan-7-one oxime
• CAS No.: 26077-63-4
• Molecular Formula: C13H27 N O
• Molecular Weight: 213.363
• Hs Code.: 2928000090
• Mol file: 26077-63-4.mol

Synonyms:NSC 338025

Chemical Property of Tridecan-7-one oxime

Chemical Property:

• Vapor Pressure: 8.63E-05mmHg at 25°C
• Boiling Point: 316.6°Cat760mmHg
• Flash Point: 192.9°C
• PSA: 32.59000
• Density: 0.88g/cm³
• LogP: 4.75740

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Tridecan-7-one oxime

There total 1 articles about Tridecan-7-one oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

tridecan-7-one (462-18-0) → tridecan-7-one oxime (26077-63-4)

Guidance literature:

With potassium hydroxide; hydroxylamine hydrochloride; In methanol; at 60 ℃; for 24h;

DOI:10.1039/b713223a

Reference yield: 63.0%

tridecan-7-one oxime (26077-63-4) → 1-hexylheptylamine (22513-16-2)

Guidance literature:

With sodium; In ethanol; for 0.5h; Heating;

DOI:10.1039/b713223a

Reference yield:

tridecan-7-one oxime (26077-63-4) → N-(1-hexylheptyl)perylene-3,4,9,10-tetracarboxylic-3,4-anhydride-9,10-imide (110590-84-6)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium-dihydrobis(2-methoxyethoxy)aluminate / toluene / 4 h / 140 °C

2: 41 percent / imidazole / 4 h / 160 °C

With 1H-imidazole; sodium bis(2-methoxyethoxy)aluminium dihydride; In toluene;

upstream raw materials:

tridecan-7-one

Downstream raw materials:

1-hexylheptylamine

N-(1-hexylheptyl)perylene-3,4,9,10-tetracarboxylic-3,4-anhydride-9,10-imide

Refernces

• 1、 Soh, Nobuaki,Ariyoshi, Tomoyuki,Fukaminato, Tuyoshi,Nakajima, Hizuru,Nakano, Koji,Imato, Toshihiko. "Swallow-tailed perylene derivative: A new tool for fluorescent imaging of lipid hydroperoxides". . p. 3762 - 3768. Retrieved 2008/10/09.