sodium 1-hydroxy-3,7-dimethyloct-6-ene-1-sulphonate

Base Information

• Chemical Name: sodium 1-hydroxy-3,7-dimethyloct-6-ene-1-sulphonate
• CAS No.: 65416-29-7
• Molecular Formula: C10H20 O4 S . Na
• Molecular Weight: 258.314
• Mol file: 65416-29-7.mol

Synonyms:6-Octene-1-sulfonicacid, 1-hydroxy-3,7-dimethyl-, monosodium salt (9CI)

Chemical Property of sodium 1-hydroxy-3,7-dimethyloct-6-ene-1-sulphonate

Chemical Property:

• PSA: 85.81000
• LogP: 2.70340

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of sodium 1-hydroxy-3,7-dimethyloct-6-ene-1-sulphonate

There total 2 articles about sodium 1-hydroxy-3,7-dimethyloct-6-ene-1-sulphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

3,7-dimethyl-oct-6-enal (106-23-0,26489-02-1) → sodium 1-hydroxy-3,7-dimethyloct-6-ene-1-sulfonate (65416-29-7)

Guidance literature:

With sodium hydrogensulfite; In ethanol; at 30 - 35 ℃; for 16h;

DOI:10.1016/j.tetlet.2014.03.046

Reference yield:

(R)-Citronellal (2385-77-5) → (+)-(R)-1-hydroxy-3,7-dimethyl-oct-6-ene-1-sulfonic acid ; sodium salt (65416-29-7)

Guidance literature:

With Methamphetamin;

Reference yield: 67.0%

(R)-<1-(1-Naphthyl)ethyl>ammonium chloride (82572-04-1) + sodium 1-hydroxy-3,7-dimethyloct-6-ene-1-sulfonate (65416-29-7) → (R)-N-(3,7-dimethyloct-6-enyl)-1-(1-naphthyl)ethylamine hydrochloride

Guidance literature:

(R)-<1-(1-Naphthyl)ethyl>ammonium chloride; sodium 1-hydroxy-3,7-dimethyloct-6-ene-1-sulfonate; With sodium cyanoborohydride; In methanol; at 20 ℃; for 20h;

With hydrogenchloride; In diethyl ether; at 0 ℃; for 13h;

DOI:10.1016/j.tetlet.2014.03.046

upstream raw materials:

3,7-dimethyl-oct-6-enal

(R)-Citronellal