Phosphorousacid, diethyl ester, sodium salt (1:1)

Base Information

• Chemical Name: Phosphorousacid, diethyl ester, sodium salt (1:1)
• CAS No.: 2303-76-6
• Molecular Formula: C₄H₁₀O₃P*Na
• Molecular Weight: 160.085
• Mol file: 2303-76-6.mol

Synonyms:Ethylsodium phosphite ((EtO)2(NaO)P) (6CI,7CI); Phosphorous acid, diethyl ester,sodium salt (8CI,9CI); Sodium ethyl phosphite, (EtO)2(NaO)P (6CI);(Diethoxyphosphinyl)sodium; Diethyl phosphite sodium salt; Diethylsodiophosphite; Diethyl sodiophosphonate; Diethyl sodium phosphite; Ethylsodium phosphite (EtO)2PONa); Sodium diethyl phosphite

Chemical Property of Phosphorousacid, diethyl ester, sodium salt (1:1)

Chemical Property:

• Boiling Point: 207°Cat760mmHg
• Flash Point: 79°C
• PSA: 55.11000
• Density: g/cm³
• LogP: 1.71680

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Phosphorousacid, diethyl ester, sodium salt (1:1)

There total 1 articles about Phosphorousacid, diethyl ester, sodium salt (1:1) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

phosphonic acid diethyl ester (762-04-9) + 1,8-dimethyl-1,4,8,11-tetraazatricyclo[9.3.1.14,8]hexadecane-1,8-diium diiodide → tetraethyl 4,11-dimethyl-1,4,8,11-tetrazacyclotetradecane-1,8-bis(methylphosphonate) (1220696-79-6) + sodium diethyl phosphite (2303-76-6,118080-94-7) + ethyl phosphite sodium salt (39148-16-8)

Guidance literature:

With sodium; In N,N-dimethyl-formamide;

DOI:10.1002/ejic.200900358

Reference yield: 80.0%

trichlorovinylbenzene (700-60-7) + sodium diethyl phosphite (2303-76-6,118080-94-7) → sodium diethyl phosphate (2870-30-6) + 1-Phenylethan-1,2,2-trisphosphonsaeurehexaethylester (103808-48-6)

Guidance literature:

In tetrahydrofuran; for 14h; Heating;

Reference yield: 63.0%

sodium diethyl phosphite (2303-76-6,118080-94-7) + benzaldehyde (100-52-7) → (E)-1,2-diphenyl-ethene (103-30-0) + sodium diethyl phosphate (2870-30-6)

Guidance literature:

In benzene; at 130 ℃; for 7h; Product distribution; sealed tube; other yield in refluxing benzene (14 h); other aromatic aldehydes; other nucleophile (diethyl 1-anilinocyclohexylphosphonate amino-anion);

upstream raw materials:

phosphonic acid diethyl ester

Downstream raw materials:

diethyl (3-chloropropyl)phosphonate

1,4-bis(diethoxyphosphinyl)butane

O,O-diethyl S-methyl phosphorothioate

sulfotep

Refernces