2H-Benzimidazol-2-one, 1,3-dihydro-5-chloro-1-methyl-3-(phenylmethyl)-

Base Information

Chemical Name:2H-Benzimidazol-2-one, 1,3-dihydro-5-chloro-1-methyl-3-(phenylmethyl)-
CAS No.:79759-63-0
Molecular Formula:C15H13ClN2O
Molecular Weight:272.7295
Hs Code.:
DSSTox Substance ID:DTXSID90229884
Wikidata:Q83110255

Synonyms:BRN 5568769;2H-Benzimidazol-2-one, 1,3-dihydro-5-chloro-1-methyl-3-(phenylmethyl)-;79759-63-0;1,3-Dihydro-5-chloro-1-methyl-3-(phenylmethyl)-2H-benzimidazol-2-one;DTXSID90229884;LS-33328

Suppliers and Price of 2H-Benzimidazol-2-one, 1,3-dihydro-5-chloro-1-methyl-3-(phenylmethyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2H-Benzimidazol-2-one, 1,3-dihydro-5-chloro-1-methyl-3-(phenylmethyl)-

Chemical Property:

Vapor Pressure:4.71E-07mmHg at 25°C
Boiling Point:413.7°Cat760mmHg
Flash Point:204°C
Density:1.315g/cm³
XLogP3:3.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:272.0716407
Heavy Atom Count:19
Complexity:343

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN1C2=C(C=C(C=C2)Cl)N(C1=O)CC3=CC=CC=C3

Technology Process of 2H-Benzimidazol-2-one, 1,3-dihydro-5-chloro-1-methyl-3-(phenylmethyl)-

There total 3 articles about 2H-Benzimidazol-2-one, 1,3-dihydro-5-chloro-1-methyl-3-(phenylmethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 79759-62-9
1-Benzyl-6-chloro-1,3-dihydro-benzoimidazol-2-one

: 74-88-4
methyl iodide

: 79759-63-0
3-benzyl-5-chloro-1-methyl-1H-benzo[d]imidazol-2(3H)-one

Guidance literature:: With sodium hydroxide; In methanol; for 10h; Ambient temperature;

Reference yield:

: 53703-95-0
N²-benzyl-4-chloro-o-phenylenediamine

: 79759-63-0
3-benzyl-5-chloro-1-methyl-1H-benzo[d]imidazol-2(3H)-one

Guidance literature:: Multi-step reaction with 3 steps

1: 71 percent / K₂CO₃ / dimethylformamide; H₂O / 0.5 h

2: 80.6 percent / EtONa / ethanol / 3 h / Heating

3: 88 percent / NaOH / methanol / 10 h / Ambient temperature

With sodium hydroxide; sodium ethanolate; potassium carbonate; In methanol; ethanol; water; N,N-dimethyl-formamide;

Reference yield:

: 79759-28-7
(2-Benzylamino-4-chloro-phenyl)-carbamic acid ethyl ester

: 79759-63-0
3-benzyl-5-chloro-1-methyl-1H-benzo[d]imidazol-2(3H)-one

Guidance literature:: Multi-step reaction with 2 steps

1: 80.6 percent / EtONa / ethanol / 3 h / Heating

2: 88 percent / NaOH / methanol / 10 h / Ambient temperature

With sodium hydroxide; sodium ethanolate; In methanol; ethanol;