(1R,2S,3R)-3-(4-hydroxybut-1-en-2-yl)-1,2-dimethylcyclopentanol

Base Information

Chemical Name:(1R,2S,3R)-3-(4-hydroxybut-1-en-2-yl)-1,2-dimethylcyclopentanol
CAS No.:121979-33-7
Molecular Formula:C₁₁H₂₀O₂
Molecular Weight:184.279
Hs Code.:

Synonyms:Cyclopentanepropanol,3-hydroxy-2,3-dimethyl-g-methylene-, [1R-(1a,2b,3b)]-; (-)-Chokol G; Chokol G

Suppliers and Price of (1R,2S,3R)-3-(4-hydroxybut-1-en-2-yl)-1,2-dimethylcyclopentanol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1R,2S,3R)-3-(4-hydroxybut-1-en-2-yl)-1,2-dimethylcyclopentanol

Chemical Property:

Vapor Pressure:0.000238mmHg at 25°C
Boiling Point:289.7°Cat760mmHg
Flash Point:132.2°C
Density:1.003g/cm³

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (1R,2S,3R)-3-(4-hydroxybut-1-en-2-yl)-1,2-dimethylcyclopentanol

There total 8 articles about (1R,2S,3R)-3-(4-hydroxybut-1-en-2-yl)-1,2-dimethylcyclopentanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 4028-58-4,4028-59-5,4028-60-8,4099-07-4,72402-00-7,73465-84-6,88980-49-8,88980-50-1,88980-51-2,114579-08-7,118354-05-5,118354-51-1,121009-85-6,121466-83-9
1,2-dimethyl-3-isopropenyl-cyclopentan-1-ol

: 121979-33-7,128241-80-5
chokol G

Guidance literature:: With dimethylaluminum chloride; In hexane; dichloromethane; at 0 - 25 ℃; for 1.5h;

Reference yield:

: 68151-47-3
methyl 2-oxo-6,6-dimethylbicyclo<3.1.0>hexane-1-carboxylate

: 121979-33-7,128241-80-5
chokol G

Guidance literature:: Multi-step reaction with 5 steps

1: 72 percent / 0.08 h / Heating

2: 80 percent / K₂CO₃ / acetone / 1 h / Heating

3: 63 percent / LiCl / hexamethylphosphoric acid triamide / 5 h / 100 °C

4: 1) CeCl₃*7H₂O / 1) THF, -78 deg C, 30 min, 2) THF, -78 deg C, 3 h

5: 55 percent / Me₂AlCl / CH₂Cl₂; hexane / 1.5 h / 0 - 25 °C

With cerium(III) chloride; dimethylaluminum chloride; potassium carbonate; lithium chloride; In N,N,N,N,N,N-hexamethylphosphoric triamide; hexane; dichloromethane; acetone;

Reference yield:

: 68151-48-4,79976-03-7,79976-04-8,85642-71-3,97690-49-8
methyl trans-2-isopropenyl-5-oxocyclopentanecarboxylate

: 121979-33-7,128241-80-5
chokol G

Guidance literature:: Multi-step reaction with 4 steps

1: 80 percent / K₂CO₃ / acetone / 1 h / Heating

2: 63 percent / LiCl / hexamethylphosphoric acid triamide / 5 h / 100 °C

3: 1) CeCl₃*7H₂O / 1) THF, -78 deg C, 30 min, 2) THF, -78 deg C, 3 h

4: 55 percent / Me₂AlCl / CH₂Cl₂; hexane / 1.5 h / 0 - 25 °C

With cerium(III) chloride; dimethylaluminum chloride; potassium carbonate; lithium chloride; In N,N,N,N,N,N-hexamethylphosphoric triamide; hexane; dichloromethane; acetone;