1,2-Benzenediol, 3,5-bis((trifluoromethyl)sulfonyl)-

Base Information

Chemical Name:1,2-Benzenediol, 3,5-bis((trifluoromethyl)sulfonyl)-
CAS No.:125629-20-1
Molecular Formula:C₈H₄F₆O₆S₂
Molecular Weight:374.239
Hs Code.:
DSSTox Substance ID:DTXSID90154824
Wikidata:Q83022174
Mol file:125629-20-1.mol

Synonyms:3,5-Bis((trifluoromethyl)sulfonyl)-1,2-benzenediol;125629-20-1;1,2-Benzenediol, 3,5-bis((trifluoromethyl)sulfonyl)-;C8H4F6O6S2;DTXSID90154824;C8-H4-F6-O6-S2;LS-29938

Suppliers and Price of 1,2-Benzenediol, 3,5-bis((trifluoromethyl)sulfonyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 1,2-Benzenediol, 3,5-bis((trifluoromethyl)sulfonyl)-

Chemical Property:

Vapor Pressure:3.96E-10mmHg at 25°C
Boiling Point:487.5°Cat760mmHg
Flash Point:248.6°C
Density:1.846g/cm³
XLogP3:2.7
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:12
Rotatable Bond Count:2
Exact Mass:373.93534916
Heavy Atom Count:22
Complexity:610

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=C(C=C(C(=C1O)O)S(=O)(=O)C(F)(F)F)S(=O)(=O)C(F)(F)F

Technology Process of 1,2-Benzenediol, 3,5-bis((trifluoromethyl)sulfonyl)-

There total 4 articles about 1,2-Benzenediol, 3,5-bis((trifluoromethyl)sulfonyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.4%

: 125629-44-9
1,2-dimethoxy-3,5-bis<(trifluoromethyl)sulfonyl>benzene

: 125629-20-1
3,5-bis<(trifluoromethyl)sulfonyl>benzene-1,2-diol

Guidance literature:: With pyridine hydrochloride; at 148 ℃; for 1h;
DOI:10.1002/hlca.19890720511

Reference yield:

: 120208-23-3
2,4-diiodo-6-methoxyphenol

: 125629-20-1
3,5-bis<(trifluoromethyl)sulfonyl>benzene-1,2-diol

Guidance literature:: Multi-step reaction with 4 steps

1: 83.4 percent / K₂CO₃ / dimethylformamide / 1 h / Ambient temperature

2: 79.7 percent / various solvent(s) / 3 h / 160 °C

3: 96.1 percent / 30percent H₂O₂ / trifluoroacetic acid / 1 h / Heating

4: 78.4 percent / pyridine*HCl / 1 h / 148 °C

With dihydrogen peroxide; pyridine hydrochloride; potassium carbonate; In N,N-dimethyl-formamide; trifluoroacetic acid;
DOI:10.1002/hlca.19890720511

Reference yield:

: 125629-42-7
1,5-diiodo-2,3-dimethoxybenzene

: 125629-20-1
3,5-bis<(trifluoromethyl)sulfonyl>benzene-1,2-diol

Guidance literature:: Multi-step reaction with 3 steps

1: 79.7 percent / various solvent(s) / 3 h / 160 °C

2: 96.1 percent / 30percent H₂O₂ / trifluoroacetic acid / 1 h / Heating

3: 78.4 percent / pyridine*HCl / 1 h / 148 °C

With dihydrogen peroxide; pyridine hydrochloride; In trifluoroacetic acid;
DOI:10.1002/hlca.19890720511