6-methyl-5,7-dihydrodibenzo[c,e]thiepinium iodide

Base Information

Chemical Name:6-methyl-5,7-dihydrodibenzo[c,e]thiepinium iodide
CAS No.:109561-74-2
Molecular Formula:C₁₅H₁₅S*I
Molecular Weight:354.255
Hs Code.:

Synonyms:5,7-Dihydro-6-methyldibenzo[c,e]thiepiniumiodide (6CI); Dibenzo[c,e]thiepinium, 5,7-dihydro-6-methyl-, iodide (9CI)

Suppliers and Price of 6-methyl-5,7-dihydrodibenzo[c,e]thiepinium iodide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6-methyl-5,7-dihydrodibenzo[c,e]thiepinium iodide

Chemical Property:

Boiling Point:°Cat760mmHg
Flash Point:°C
Density:g/cm³

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 6-methyl-5,7-dihydrodibenzo[c,e]thiepinium iodide

There total 4 articles about 6-methyl-5,7-dihydrodibenzo[c,e]thiepinium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 6672-64-6
5,7-dihydrodibenzo[c,e]thiepine

: 74-88-4
methyl iodide

: 109561-74-2
6-methyl-5,7-dihydrodibenzothiepinium iodide

Guidance literature:: In ethanol; for 8h; Heating;

Reference yield:

: 38274-14-5
2,2'-bis-(bromomethyl)-1,1'-biphenyl

: 109561-74-2
6-methyl-5,7-dihydrodibenzothiepinium iodide

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / Na₂S*9H₂O / H₂O; methanol / Heating

2: 76 percent / ethanol / 8 h / Heating

With sodium sulfide; In methanol; ethanol; water;

Reference yield:

: 863305-32-2
diphenic acid

: 109561-74-2
6-methyl-5,7-dihydrodibenzothiepinium iodide

Guidance literature:: Multi-step reaction with 4 steps

1: 73 percent / NaBH₄, BF₃*O(C₂H₅)2 / tetrahydrofuran

2: 98 percent / HBr / H₂O; H₂SO₄ / Heating

3: 84 percent / Na₂S*9H₂O / H₂O; methanol / Heating

4: 76 percent / ethanol / 8 h / Heating

With sodium sulfide; sodium tetrahydroborate; boron trifluoride diethyl etherate; hydrogen bromide; In tetrahydrofuran; methanol; ethanol; sulfuric acid; water;