(6-Methyl-5-nitropyridin-2-yl)hydrazine

Base Information

Chemical Name:(6-Methyl-5-nitropyridin-2-yl)hydrazine
CAS No.:28489-37-4
Molecular Formula:C₆H₈N₄O₂
Molecular Weight:168.155
Hs Code.:
DSSTox Substance ID:DTXSID70401580
NSC Number:170623
Wikidata:Q82204760
Mol file:28489-37-4.mol

Synonyms:28489-37-4;(6-methyl-5-nitropyridin-2-yl)hydrazine;Pyridine, 6-hydrazinyl-2-methyl-3-nitro-;2-Hydrazino-6-methyl-5-nitropyridine;NSC170623;SCHEMBL15167574;DTXSID70401580;6-hydrazinyl-2-methyl-3-nitropyridine;AKOS006340238;AKOS016362940;NSC-170623

Suppliers and Price of (6-Methyl-5-nitropyridin-2-yl)hydrazine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of (6-Methyl-5-nitropyridin-2-yl)hydrazine

Chemical Property:

Vapor Pressure:0.000118mmHg at 25°C
Boiling Point:335.6°Cat760mmHg
Flash Point:156.8°C
Density:1.432g/cm³
XLogP3:0.7
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:1
Exact Mass:168.06472551
Heavy Atom Count:12
Complexity:169

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(C=CC(=N1)NN)[N+](=O)[O-]

Technology Process of (6-Methyl-5-nitropyridin-2-yl)hydrazine

There total 4 articles about (6-Methyl-5-nitropyridin-2-yl)hydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 22280-60-0
6-chloro-4-methyl-3-nitropyridine

: 28489-37-4
(6-methyl-5-nitro-[2]pyridyl)-hydrazine

Guidance literature:: With ethanol; sodium acetate; hydrazine hydrate;
DOI:10.1021/ja01135a033

Reference yield:

: 28489-45-4
6-methyl-5-nitropyridin-2-ol

: 28489-37-4
(6-methyl-5-nitro-[2]pyridyl)-hydrazine

Guidance literature:: Multi-step reaction with 2 steps

1: phosphorus (V)-chloride; phosphoryl chloride

2: sodium acetate; ethanol; N₂H₄+H₂O

With ethanol; phosphorus pentachloride; sodium acetate; hydrazine hydrate; trichlorophosphate;
DOI:10.1021/ja01135a033

Reference yield:

: 22280-62-2
6-methyl-5-nitro-2-pyridinamine

: 28489-37-4
(6-methyl-5-nitro-[2]pyridyl)-hydrazine

Guidance literature:: Multi-step reaction with 3 steps

1: aqueous sodium nitrite; aqueous sulfuric acid / Diazotization

2: phosphorus (V)-chloride; phosphoryl chloride

3: sodium acetate; ethanol; N₂H₄+H₂O

With ethanol; phosphorus pentachloride; sulfuric acid; sodium acetate; hydrazine hydrate; sodium nitrite; trichlorophosphate;
DOI:10.1021/ja01135a033