b-D-Glucopyranoside,2-(cis-1,4-dihydroxycyclohexyl)ethyl (9CI)

Base Information

Chemical Name:b-D-Glucopyranoside,2-(cis-1,4-dihydroxycyclohexyl)ethyl (9CI)
CAS No.:101489-32-1
Molecular Formula:C14H26 O8
Molecular Weight:322.356
Hs Code.:
Mol file:101489-32-1.mol

Synonyms:b-D-Glucopyranoside,2-(1,4-dihydroxycyclohexyl)ethyl, cis-; Rengyoside A

Suppliers and Price of b-D-Glucopyranoside,2-(cis-1,4-dihydroxycyclohexyl)ethyl (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of b-D-Glucopyranoside,2-(cis-1,4-dihydroxycyclohexyl)ethyl (9CI)

Chemical Property:

Purity/Quality:: 98%min ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of b-D-Glucopyranoside,2-(cis-1,4-dihydroxycyclohexyl)ethyl (9CI)

There total 6 articles about b-D-Glucopyranoside,2-(cis-1,4-dihydroxycyclohexyl)ethyl (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 101489-37-6
(2R,3R,4S,5S,6R)-2-[2-(1-Hydroxy-4,4-dimethoxy-cyclohexyl)-ethoxy]-6-hydroxymethyl-tetrahydro-pyran-3,4,5-triol

: 101489-32-1
rengyoside A

Guidance literature:: With sodium cyanoborohydride; In acetic acid; for 0.5h; Ambient temperature; pH = 4;
DOI:10.1016/S0040-4020(01)89229-2

Reference yield:

: 40661-45-8
cornoside

: 101489-32-1
rengyoside A

Guidance literature:: Multi-step reaction with 2 steps

1: 21 percent / hydrogen / 5percent Pd/C / methanol / 6 h / 80 °C / 7600 Torr

2: 70 percent / NaBH₃CN / aq. acetic acid / 0.5 h / Ambient temperature; pH = 4

With hydrogen; sodium cyanoborohydride; palladium on activated charcoal; In methanol; acetic acid;
DOI:10.1016/S0040-4020(01)89229-2

Reference yield:

: 572-09-8
2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl bromide

: 101489-32-1
rengyoside A

Guidance literature:: Multi-step reaction with 5 steps

1: 74 percent / Ag₂CO₃ / benzene; diethyl ether / 12.5 h / Ambient temperature

2: 100 percent / K₂CO₃, MeOH

3: 1.) rose bengal, O₂, 2.) Me₂S / 1.) MeOH, irradiation, 19 h, 0 deg C

4: 21 percent / hydrogen / 5percent Pd/C / methanol / 6 h / 80 °C / 7600 Torr

5: 70 percent / NaBH₃CN / aq. acetic acid / 0.5 h / Ambient temperature; pH = 4

With methanol; dimethylsulfide; hydrogen; oxygen; rose bengal; sodium cyanoborohydride; potassium carbonate; silver carbonate; palladium on activated charcoal; In methanol; diethyl ether; acetic acid; benzene;
DOI:10.1016/S0040-4020(01)89229-2