Technology Process of CID 11809239
There total 11 articles about CID 11809239 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 73 percent / 1N aq. NaOH / tetrahydrofuran / 1 h / Ambient temperature
2: 1.) Ag2CO3, Drierite, 2.) I2 / 1.) Et2O, RT, 10 min, 2.) Et2O, RT, 14 h
3: 97.7 percent / NaOMe / methanol / 1 h / Ambient temperature
4: 1.) O2, 2.) Me2S / 1.) MeOH, 20 deg C, irrad., 3 h, 2.) MeOH, 4 h
With
calcium sulfate; sodium hydroxide; dimethylsulfide; iodine; oxygen; sodium methylate; silver carbonate;
In
tetrahydrofuran; methanol;
DOI:10.1248/cpb.46.581
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 11.5 percent / aq. thallium triperchlorate / CH2Cl2 / 0.25 h
2: 61.1 percent / NaOMe / methanol
With
thallium(III) perchlorate; sodium methylate;
In
methanol; dichloromethane;
DOI:10.1248/cpb.46.581
