N-[3-(diethylamino)propyl]-3-methyl-4-nitrobenzamide

Base Information

Chemical Name:N-[3-(diethylamino)propyl]-3-methyl-4-nitrobenzamide
CAS No.:5649-79-6
Molecular Formula:C15H23N3O3
Molecular Weight:238.373
Hs Code.:2902909090
DSSTox Substance ID:DTXSID70366741
Wikidata:Q82152118

Synonyms:5649-79-6;ST50687377;DTXSID70366741;AKOS000678085

Suppliers and Price of N-[3-(diethylamino)propyl]-3-methyl-4-nitrobenzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of N-[3-(diethylamino)propyl]-3-methyl-4-nitrobenzamide

Chemical Property:

Vapor Pressure:1.13E-07mmHg at 25°C
Melting Point:120-120.5 °C
Boiling Point:432.2°C at 760 mmHg
Flash Point:215.2°C
PSA：78.16000
Density:1.11g/cm³
LogP:3.27900
XLogP3:2.5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:7
Exact Mass:293.17394160
Heavy Atom Count:21
Complexity:340

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCN(CC)CCCNC(=O)C1=CC(=C(C=C1)[N+](=O)[O-])C

Technology Process of N-[3-(diethylamino)propyl]-3-methyl-4-nitrobenzamide

There total 9 articles about N-[3-(diethylamino)propyl]-3-methyl-4-nitrobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 74-85-1
ethene

: 624-31-7
4-tolyl iodide

: 5649-79-6
4,4'-(butane-2,3-diyl)bis(methylbenzene)

Guidance literature:: With nickel(II) iodide; N,N,N,N,-tetramethylethylenediamine; (4,4'-di-tert-butyl-2,2'-dipyridyl)-bis-(2-phenylpyridine(-1H))-iridium(III) hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In dimethyl sulfoxide; at 100 ℃; for 24h; under 12929 Torr; Reagent/catalyst; Schlenk technique; Sealed tube; Irradiation;
DOI:10.1016/j.chempr.2018.10.006

Reference yield: 89.0%

: 74-85-1
ethene

: 106-38-7
para-bromotoluene

: 5649-79-6
4,4'-(butane-2,3-diyl)bis(methylbenzene)

Guidance literature:: With nickel(II) iodide; N,N,N,N,-tetramethylethylenediamine; (4,4'-di-tert-butyl-2,2'-dipyridyl)-bis-(2-phenylpyridine(-1H))-iridium(III) hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In dimethyl sulfoxide; at 100 ℃; for 24h; under 12929 Torr; Schlenk technique; Sealed tube; Irradiation;
DOI:10.1016/j.chempr.2018.10.006

Reference yield: 80.0%

: 622-97-9,24936-41-2
1-ethenyl-4-methylbenzene

: 622-96-8
4-methylethylbenzene

: 5649-79-6
4,4'-(butane-2,3-diyl)bis(methylbenzene)

Guidance literature:: With titanium(III) citrate; Tris buffer; tetra(n-butyl)ammonium hydroxide; vitamin B-12; In ethanol; pH=8;
DOI:10.1021/jo0160470