Dipropylamine, N-nitro-

Base Information

• Chemical Name: Dipropylamine, N-nitro-
• CAS No.: 4164-29-8
• Molecular Formula: C6H14N2O2
• Molecular Weight: 146.189
• NSC Number: 137910,137897
• DSSTox Substance ID: DTXSID60194454
• Wikidata: Q83067199
• Mol file: 4164-29-8.mol

Synonyms:Di-n-propylnitramine;Dipropylamine, N-nitro-;Dipropylnitramine;1-Propanamine, N-nitro-N-propyl-;4164-29-8;NSC137910;DTXSID60194454;NSC137897;NSC 137897;NSC 137910;NSC-137897;NSC-137910;1-Oxo-2,2-dipropylhydrazine 1-oxide #

Chemical Property of Dipropylamine, N-nitro-

Chemical Property:

• Vapor Pressure: 0.0481mmHg at 25°C
• Boiling Point: 244.2°Cat760mmHg
• Flash Point: 101.5°C
• Density: 0.99g/cm³
• XLogP3: 2.4
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 4
• Exact Mass: 146.105527694
• Heavy Atom Count: 10
• Complexity: 94.4

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCCN(CCC)[N+](=O)[O-]

Technology Process of Dipropylamine, N-nitro-

There total 5 articles about Dipropylamine, N-nitro- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

dipropylammonium nitrate (67559-82-4) → N-nitroso-N,N-dipropylamine (621-64-7) + N-nitrodipropylamine (4164-29-8)

Guidance literature:

With nitric acid; acetic anhydride; zinc(II) chloride; In carbon dioxide; at 20 ℃; for 24h; under 45004.5 - 60006 Torr; Autoclave;

DOI:10.1007/s11172-009-0282-1

Reference yield:

N,N-dipropylcarbamoyl chloride (27086-19-7) → N-nitroso-N,N-dipropylamine (621-64-7) + N-nitrodipropylamine (4164-29-8)

Guidance literature:

With tetrachloromethane; silver nitrate;

DOI:10.1021/ja01522a047

Reference yield:

tetrachloromethane (56-23-5) + silver nitrate + N,N-dipropylcarbamoyl chloride (27086-19-7) → N-nitroso-N,N-dipropylamine (621-64-7) + N-nitrodipropylamine (4164-29-8) + dipropylammonium nitrate (67559-82-4)

Guidance literature:

at 60 ℃;

DOI:10.1021/ja01522a047

upstream raw materials:

N,N-dipropylcarbamoyl chloride

N-nitroso-N,N-dipropylamine

tetrachloromethane

acetonitrile

Downstream raw materials:

N-nitroso-N,N-dipropylamine