3-(2-(1,3-Dioxo-2-phenyl-4,5,6,7-tetrahydro-4,7-dithiaindanyl))glutarimide

Base Information

Chemical Name:3-(2-(1,3-Dioxo-2-phenyl-4,5,6,7-tetrahydro-4,7-dithiaindanyl))glutarimide
CAS No.:76059-14-8
Molecular Formula:C18H15 N O4 S2
Molecular Weight:373.46
Hs Code.:
DSSTox Substance ID:DTXSID50997390
Mol file:76059-14-8.mol

Synonyms:BRN 6000295;76059-14-8;3-(2-(1,3-Dioxo-2-phenyl-4,5,6,7-tetrahydro-4,7-dithiaindanyl))glutarimide;Glutarimide, 3-(5,7-dioxo-6-phenyl-2,3,6,7-tetrahydro-5H-cyclopenta-p-dithiin-6-yl)-;DTXSID50997390;LS-72059;6-(6-Hydroxy-2-oxo-2,3,4,5-tetrahydropyridin-3-yl)-6-phenyl-2,3-dihydro-5H-cyclopenta[b][1,4]dithiine-5,7(6H)-dione

Suppliers and Price of 3-(2-(1,3-Dioxo-2-phenyl-4,5,6,7-tetrahydro-4,7-dithiaindanyl))glutarimide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
3-(2-(1,3-DIOXO-2-PHENYL-4,5,6,7-TETRAHYDRO-4,7-DITHIAINDANYL))GLUTARIMIDE 95.00%
5MG
$ 503.23

Total 5 raw suppliers

Chemical Property of 3-(2-(1,3-Dioxo-2-phenyl-4,5,6,7-tetrahydro-4,7-dithiaindanyl))glutarimide

Chemical Property:

Vapor Pressure:5.55E-17mmHg at 25°C
Refractive Index:1.7000 (estimate)
Boiling Point:654°C at 760 mmHg
Flash Point:349.3°C
PSA：134.40000
Density:1.5g/cm³
LogP:2.09650
XLogP3:1.8
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:2
Exact Mass:373.04425031
Heavy Atom Count:25
Complexity:665

Purity/Quality:

99% ^*data from raw suppliers

3-(2-(1,3-DIOXO-2-PHENYL-4,5,6,7-TETRAHYDRO-4,7-DITHIAINDANYL))GLUTARIMIDE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CC(=O)NC(=O)C1C2(C(=O)C3=C(C2=O)SCCS3)C4=CC=CC=C4

Technology Process of 3-(2-(1,3-Dioxo-2-phenyl-4,5,6,7-tetrahydro-4,7-dithiaindanyl))glutarimide

There total 2 articles about 3-(2-(1,3-Dioxo-2-phenyl-4,5,6,7-tetrahydro-4,7-dithiaindanyl))glutarimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 7747-10-6
2-Phenyl-4,5,6,7-tetrahydro-4,7-dithia-1,3-indandion

: 62595-74-8
3-bromopiperidine-2,6-dione

: 76059-14-8
3-<2-(1,3-Dioxo-2-phenyl-4,5,6,7-tetrahydro-4,7-dithiaindanyl)>glutarimid

Guidance literature:: With sodium; 1.) EtOH, 2.) THF, reflux, 1 h;
DOI:10.1002/ardp.19803130602

Reference yield:

: 10489-75-5
5,6-dihydro-1,4-dithiin-2,3-dicarboxylic anhydride

: 76059-14-8
3-<2-(1,3-Dioxo-2-phenyl-4,5,6,7-tetrahydro-4,7-dithiaindanyl)>glutarimid

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / acetanhydride, triethylamine / 2 h / Heating

2: 78 percent / 1.) Na / 1.) EtOH, 2.) THF, reflux, 1 h

With sodium; acetic anhydride; triethylamine;
DOI:10.1002/ardp.19803130602