1-chloro-8-nitroanthracene-9,10-dione

Base Information

• Chemical Name: 1-chloro-8-nitroanthracene-9,10-dione
• CAS No.: 129-38-4
• Molecular Formula: C₁₄H₆ClNO₄
• Molecular Weight: 287.659
• Mol file: 129-38-4.mol

Synonyms:Anthraquinone,1-chloro-8-nitro- (6CI,8CI); 1-Chloro-8-nitroanthraquinone;1-Nitro-8-chloroanthraquinone; 8-Chloro-1-nitroanthraquinone; NSC 15365

Chemical Property of 1-chloro-8-nitroanthracene-9,10-dione

Chemical Property:

• Vapor Pressure: 1.85E-10mmHg at 25°C
• Boiling Point: 508.5°Cat760mmHg
• Flash Point: 261.3°C
• Density: 1.573g/cm³

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-chloro-8-nitroanthracene-9,10-dione

There total 7 articles about 1-chloro-8-nitroanthracene-9,10-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

potassium 8-nitroanthraquinone-1-sulfonate → 8-chloro-1-nitroanthraquinone (129-38-4)

Guidance literature:

With hydrogenchloride; sodium chlorate; for 1h; Heating;

DOI:10.1021/jm010041l

Reference yield:

1,8-dinitroanthraquinone (129-39-5) + ammonium chloride → 8-chloro-1-nitroanthraquinone (129-38-4)

Guidance literature:

With lithium chloride; In sulfolane;

Reference yield:

→ 8-chloro-1-nitroanthraquinone (129-38-4)

Guidance literature:

With thionyl chloride; at 170 ℃;

upstream raw materials:

8-nitro-9,10-dioxo-9,10-dihydro-anthracene-1-sulfonic acid

hydrogenchloride

1,8-dinitroanthraquinone