1-Naphthalenemethanimine, alpha-(2,3-dihydro-7-methyl-1H-inden-4-yl)-, hydrochloride

Base Information

• Chemical Name: 1-Naphthalenemethanimine, alpha-(2,3-dihydro-7-methyl-1H-inden-4-yl)-, hydrochloride
• CAS No.: 63549-35-9
• Molecular Formula: C₂₁H₁₉N*ClH
• Molecular Weight: 321.85
• DSSTox Substance ID: DTXSID3069930

Synonyms:63549-35-9;1-(7-Methyl-4-indanyl)-1-(1-naphthyl)methanimine, hydrochloride;1-Naphthalenemethanimine, .alpha.-(2,3-dihydro-7-methyl-1H-inden-4-yl)-, hydrochloride;1-Naphthalenemethanimine, alpha-(2,3-dihydro-7-methyl-1H-inden-4-yl)-, hydrochloride;1-Naphthalenemethanimine, alpha-(2,3-dihydro-7-methyl-1H-inden-4-yl)-, hydrochloride (1:1);DTXSID3069930

Chemical Property of 1-Naphthalenemethanimine, alpha-(2,3-dihydro-7-methyl-1H-inden-4-yl)-, hydrochloride

Chemical Property:

• Vapor Pressure: 3.04E-08mmHg at 25°C
• Boiling Point: 461.1°Cat760mmHg
• Flash Point: 232.6°C
• Density: g/cm³
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 2
• Exact Mass: 321.1284273
• Heavy Atom Count: 23
• Complexity: 414

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=C2CCCC2=C(C=C1)C(=N)C3=CC=CC4=CC=CC=C43.Cl

Technology Process of 1-Naphthalenemethanimine, alpha-(2,3-dihydro-7-methyl-1H-inden-4-yl)-, hydrochloride

There total 1 articles about 1-Naphthalenemethanimine, alpha-(2,3-dihydro-7-methyl-1H-inden-4-yl)-, hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-Bromonaphthalene (90-11-9) + 4-Cyano-7-methylhydrindene (15085-20-8) → 7-Methylindan-4-yl 1-naphthyl ketimine hydrochloride (63549-35-9)

Guidance literature:

With magnesium; Yield given. Multistep reaction; 1.) THF, 66 deg C, 2.) reflux, 4 h;

DOI:10.1021/jo00330a008

Reference yield: 75.0%

7-Methylindan-4-yl 1-naphthyl ketimine hydrochloride (63549-35-9) → (7-methyl-indan-4-yl)-[1]naphthyl ketone (63665-87-2)

Guidance literature:

With hydrogenchloride; acetic acid; In xylene; for 4h; Heating;

DOI:10.1021/jo00330a008

upstream raw materials:

1-Bromonaphthalene

4-Cyano-7-methylhydrindene

Downstream raw materials:

(7-methyl-indan-4-yl)-[1]naphthyl ketone

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