3-Bromo-2-decalone

Base Information

• Chemical Name: 3-Bromo-2-decalone
• CAS No.: 5710-07-6
• Molecular Formula: C₁₀H₁₅BrO
• Molecular Weight: 231.132
• NSC Number: 117436
• DSSTox Substance ID: DTXSID10297707
• Mol file: 5710-07-6.mol

Synonyms:3-Bromo-2-decalone;5710-07-6;3-bromooctahydronaphthalen-2(1h)-one;NSC117436;DTXSID10297707;NSC-117436;2(1H)-Naphthalenone, 3-bromooctahydro-

Chemical Property of 3-Bromo-2-decalone

Chemical Property:

• Vapor Pressure: 0.00209mmHg at 25°C
• Boiling Point: 290.3°Cat760mmHg
• Flash Point: 67.5°C
• Density: 1.365g/cm³
• XLogP3: 3.4
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 0
• Exact Mass: 230.03063
• Heavy Atom Count: 12
• Complexity: 190

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: C1CCC2CC(=O)C(CC2C1)Br

Technology Process of 3-Bromo-2-decalone

There total 13 articles about 3-Bromo-2-decalone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(4aR,8aR)-3-Bromo-decahydro-naphthalen-2-ol → 3-bromo-trans-decalin-2-one (3849-23-8,5710-07-6,21399-55-3,21399-58-6,21441-82-7,28051-63-0,29293-31-0)

Guidance literature:

With jones reagent; In acetone; at 7 - 10 ℃;

DOI:10.1021/jo00242a015

Reference yield:

trans-decalin-2-one (4832-17-1,5779-29-3,5779-30-6,16021-08-2,52079-67-1,91684-29-6,91684-30-9,1579-21-1,143392-76-1) → 3-bromo-trans-decalin-2-one (3849-23-8,5710-07-6,21399-55-3,21399-58-6,21441-82-7,28051-63-0,29293-31-0)

Guidance literature:

With bromine; In acetic acid;

DOI:10.1021/jm00295a031

Reference yield:

trans-decalin-2-one (4832-17-1,5779-29-3,5779-30-6,16021-08-2,52079-67-1,91684-29-6,91684-30-9,1579-21-1,143392-76-1) → rac.-3α-Brom-4a α H-trans-decalon-(2) (3849-23-8,5710-07-6,21399-55-3,21399-58-6,21441-82-7,28051-63-0,29293-31-0)

Guidance literature:

With bromine; In chloroform; acetic acid;

DOI:10.1021/jm00322a002

upstream raw materials:

trans-decalin-2-one

rel-(4aS,8aS)-1,2,3,4,4a,5,8,8a-octahydronaphthalen-2-one

trans-2,3-octalin

rac.-3α-Brom-4a α H-trans-decalon-(2)

Downstream raw materials:

3-methylbenzonaphtho<2,3-d>thiophene

1-methylbenzonaphtho<2,3-d>thiophene

3-(p-methylphenylthio)-2-decalone

4-methyl-benzo[b]naphtho[2,3-d]thiophene