3-(p-methylphenylthio)-2-decalone

Base Information

• Chemical Name: 3-(p-methylphenylthio)-2-decalone
• CAS No.: 83656-91-1
• Molecular Formula: C₁₇H₂₂OS
• Molecular Weight: 274.427
• Mol file: 83656-91-1.mol

Synonyms:

Chemical Property of 3-(p-methylphenylthio)-2-decalone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 3-(p-methylphenylthio)-2-decalone

There total 1 articles about 3-(p-methylphenylthio)-2-decalone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-bromo-2-decalone (5710-07-6) + para-thiocresol (106-45-6) → 3-(p-methylphenylthio)-2-decalone (83656-91-1)

Guidance literature:

In pyridine; 1.) 25-30 deg C, 15 min, 2.) 100 deg C, 2 h.;

Reference yield:

3-(p-methylphenylthio)-2-decalone (83656-91-1) → 2-methylbenzonaphtho<2,3-d>thiophene (83656-84-2)

Guidance literature:

Multi-step reaction with 2 steps

1: polyphosphoric acid / 3 h / Heating

2: powdered selenium / 8 h / 300 °C

With selenium; PPA;

upstream raw materials:

3-bromo-2-decalone

para-thiocresol

Downstream raw materials:

2-methylbenzonaphtho<2,3-d>thiophene