1-(2,3-Dideoxy-alpha-D-erythro-hex-2-enopyranosyl)-2-nitro-1H-imidazole

Base Information

Chemical Name:1-(2,3-Dideoxy-alpha-D-erythro-hex-2-enopyranosyl)-2-nitro-1H-imidazole
CAS No.:82205-95-6
Molecular Formula:C₉H₁₁N₃O₅
Molecular Weight:241.203
Hs Code.:
NSC Number:364383,342714
DSSTox Substance ID:DTXSID501002553
Mol file:82205-95-6.mol

Synonyms:1-(2',3'-dideoxy-alpha-D-erythro-hex-2'-enopyranosyl)-2-nitroimidazole;RA 263;RA-263

Suppliers and Price of 1-(2,3-Dideoxy-alpha-D-erythro-hex-2-enopyranosyl)-2-nitro-1H-imidazole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
1-(2,3-DIDEOXY-ALPHA-D-ERYTHRO-HEX-2-ENOPYRANOSYL)-2-NITRO-1H-IMIDAZOLE 95.00%
5MG
$ 496.83

Total 5 raw suppliers

Chemical Property of 1-(2,3-Dideoxy-alpha-D-erythro-hex-2-enopyranosyl)-2-nitro-1H-imidazole

Chemical Property:

Vapor Pressure:2.12E-13mmHg at 25°C
Boiling Point:560.5°C at 760 mmHg
Flash Point:292.8°C
PSA：113.33000
Density:1.69g/cm³
LogP:0.12130
XLogP3:-0.2
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:2
Exact Mass:241.06987046
Heavy Atom Count:17
Complexity:318

Purity/Quality:: 1-(2,3-DIDEOXY-ALPHA-D-ERYTHRO-HEX-2-ENOPYRANOSYL)-2-NITRO-1H-IMIDAZOLE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(OC(C1O)CO)N2C=CN=C2[N+](=O)[O-]

Technology Process of 1-(2,3-Dideoxy-alpha-D-erythro-hex-2-enopyranosyl)-2-nitro-1H-imidazole

There total 3 articles about 1-(2,3-Dideoxy-alpha-D-erythro-hex-2-enopyranosyl)-2-nitro-1H-imidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.3%

: 83416-43-7
Acetic acid (2R,3S,6S)-2-acetoxymethyl-6-(2-nitro-imidazol-1-yl)-3,6-dihydro-2H-pyran-3-yl ester

: 82205-95-6
1-(2',3'-dideoxy-α-D-erythro-hex-2'-enopyranosyl)-2-nitroimidazole

Guidance literature:: With ammonia; at 0 ℃;
DOI:10.1021/jm00355a005

Reference yield:

: 69515-91-9
1,3,4,6-tetra-O-acetyl-2-deoxy-D-glucopyranose

: 82205-95-6
1-(2',3'-dideoxy-α-D-erythro-hex-2'-enopyranosyl)-2-nitroimidazole

Guidance literature:: Multi-step reaction with 2 steps

1: 5.2 percent / SnCl₄ / CH₂Cl₂ / 0.75 h / 60 - 70 °C

2: 66.3 percent / sat. methanol. NH₃ / 0 °C

With ammonia; tin(IV) chloride; In dichloromethane;
DOI:10.1021/jm00355a005

Reference yield:

: 2873-29-2
D-glucal triacetate

: 82205-95-6
1-(2',3'-dideoxy-α-D-erythro-hex-2'-enopyranosyl)-2-nitroimidazole

Guidance literature:: Multi-step reaction with 2 steps

1: 2.) ZnCl₂ / 1.) from 90 to 100 deg C, 10 min, vacuum, 2.) from 140 to 160 deg C, 45 min, vacuum

2: 66.3 percent / sat. methanol. NH₃ / 0 °C

With ammonia; zinc(II) chloride;
DOI:10.1021/jm00355a005