N-(3-chlorobenzyl)-N-propylamine

Base Information

• Chemical Name: N-(3-chlorobenzyl)-N-propylamine
• CAS No.: 39190-98-2
• Molecular Formula: C10H14ClN
• Molecular Weight: 183.681
• Hs Code.: 2921499090
• Mol file: 39190-98-2.mol

Synonyms:(m-Chlorobenzyl)propylamine;N-(3-chlorobenzyl)-N-propylamine;(3-Chlorobenzyl)propylamine;N-(3-Chlorophenylmethyl)propylamine;

Chemical Property of N-(3-chlorobenzyl)-N-propylamine

Chemical Property:

• Vapor Pressure: 0.0282mmHg at 25°C
• Refractive Index: 1.52
• Boiling Point: 245.8 °C at 760 mmHg
• Flash Point: 102.4 °C
• PSA: 12.03000
• Density: 1.043 g/cm³
• LogP: 3.23050

Purity/Quality:

99.90% ^*data from raw suppliers

(m-Chlorobenzyl)propylamine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: (m-Chlorobenzyl)propylamine acts as a reagent in the preparation of novel dimethoxy-N2-(substituted benzyl)-N2-propylquinazoline diamine derivatives as anxiolytic and antidepressant agents

Technology Process of N-(3-chlorobenzyl)-N-propylamine

There total 2 articles about N-(3-chlorobenzyl)-N-propylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

propylamine (107-10-8,42939-71-9) + m-Chlorobenzaldehyde (587-04-2) → N-(3-chlorobenzyl)propylamine (39190-98-2)

Guidance literature:

propylamine; m-Chlorobenzaldehyde; In methanol; at 0 - 20 ℃; for 3.5h;

With sodium tetrahydroborate; In methanol; at 0 - 20 ℃;

Reference yield:

[1-(3-Chloro-phenyl)-meth-(E)-ylidene]-propyl-amine (1032080-61-7) → N-(3-chlorobenzyl)propylamine (39190-98-2)

Guidance literature:

With lithium aluminium tetrahydride; In diethyl ether; for 2h; Heating;

DOI:10.1021/jm00375a005

Reference yield: 70.0%

4-chloro-2-phenylquinazoline (6484-25-9) + N-(3-chlorobenzyl)propylamine (39190-98-2) → C24H22ClN3

Guidance literature:

Reflux;

upstream raw materials:

[1-(3-Chloro-phenyl)-meth-(E)-ylidene]-propyl-amine

propylamine

m-Chlorobenzaldehyde

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