1,2-diphenylethanaminium chloride

Base Information

Chemical Name:1,2-diphenylethanaminium chloride
CAS No.:14149-00-9
Molecular Formula:C₁₄H₁₅N*ClH
Molecular Weight:233.741
Hs Code.:

Synonyms:Benzeneethanamine,a-phenyl-, hydrochloride, (S)-(9CI); Ethylamine, 1,2-diphenyl-, hydrochloride, (S)-(+)- (8CI);(S)-1,2-Diphenylethylamine hydrochloride

Suppliers and Price of 1,2-diphenylethanaminium chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 1,2-diphenylethanaminium chloride

Chemical Property:

Vapor Pressure:0.000575mmHg at 25°C
Boiling Point:311.1°Cat760mmHg
Flash Point:136.8°C
Density:g/cm³

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1,2-diphenylethanaminium chloride

There total 10 articles about 1,2-diphenylethanaminium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: phenylmagnesium bromide

: 221375-48-0
(N(E),R)-2-methyl-N-(2-phenylethylidene)-2-propanesulfinamide

: 14149-01-0,24301-89-1
(R)-1,2-diphenylethylamine hydrochloride

: 14149-00-9,24301-89-1
(S)-1,2-diphenylethylamine hydrochloride

Guidance literature:: phenylmagnesium bromide; (N(E),R)-2-methyl-N-(2-phenylethylidene)-2-propanesulfinamide; In diethyl ether; dichloromethane; at -48 ℃;

With hydrogenchloride; In 1,4-dioxane; methanol; at 20 ℃; for 0.5h; Title compound not separated from byproducts; Solvolysis;
DOI:10.1016/S0040-4020(99)00451-2

Reference yield:

: 100-46-9
benzylamine

: 14149-00-9,24301-89-1
(S)-1,2-diphenylethylamine hydrochloride

Guidance literature:: Multi-step reaction with 5 steps

1: 93 percent / BF₃*Et₂O / benzene / 4 h / Heating; Cope apparatus (4 Angstroem molecular sieves)

2: n-butyllithium / tetrahydrofuran; hexane / 6 h / -78 °C / other temperature

3: hydroxylamine hydrochloride, AcONa*3H₂O / ethanol / 19 h / Ambient temperature

4: dioxane / 4 h / Ambient temperature

5: 10percent HCl-MeOH / Ambient temperature

With hydrogenchloride; n-butyllithium; boron trifluoride diethyl etherate; hydroxylamine hydrochloride; sodium acetate; In tetrahydrofuran; 1,4-dioxane; ethanol; hexane; benzene;
DOI:10.1016/0040-4020(95)00828-V

Reference yield:

: 3082-58-4
(S)-1,2-diphenylethyl amine

: 14149-00-9,24301-89-1
(S)-1,2-diphenylethylamine hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: dioxane / 4 h / Ambient temperature

2: 10percent HCl-MeOH / Ambient temperature

With hydrogenchloride; In 1,4-dioxane;
DOI:10.1016/0040-4020(95)00828-V