2,5-Dimethylhex-1-en-3-ol

Base Information

Chemical Name:2,5-Dimethylhex-1-en-3-ol
CAS No.:77722-56-6
Molecular Formula:C8H16O
Molecular Weight:128.212
Hs Code.:
NSC Number:107261
DSSTox Substance ID:DTXSID00296047
Nikkaji Number:J2.221.537J

Synonyms:77722-56-6;2,5-dimethylhex-1-en-3-ol;NSC107261;DTXSID00296047;AKOS017729123;NSC-107261

Suppliers and Price of 2,5-Dimethylhex-1-en-3-ol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 2,5-Dimethylhex-1-en-3-ol

Chemical Property:

Vapor Pressure:0.938mmHg at 25°C
Boiling Point:158.3°Cat760mmHg
Flash Point:55.8°C
Density:0.833g/cm³
XLogP3:2.5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:3
Exact Mass:128.120115130
Heavy Atom Count:9
Complexity:94.7

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(C)CC(C(=C)C)O

Technology Process of 2,5-Dimethylhex-1-en-3-ol

There total 5 articles about 2,5-Dimethylhex-1-en-3-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 557-93-7
2-bromoprop-1-ene

: 590-86-3
isovaleraldehyde

: 77722-56-6
3-hydroxy-2,5-dimethyl-1-hexene

Guidance literature:: 2-bromoprop-1-ene; With magnesium; In tetrahydrofuran; for 0.5h; Reflux; Inert atmosphere;

isovaleraldehyde; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1002/chem.201100843

Reference yield:

: 78-85-3,25120-30-3
2-methylpropenal

: 77722-56-6
3-hydroxy-2,5-dimethyl-1-hexene

Guidance literature:: In tetrahydrofuran; at 0 - 20 ℃; for 0.5h; Inert atmosphere;
DOI:10.1039/c7cc01423f

Reference yield:

: 85589-70-4
1-chloro-3-methyl-but-3-en-2-ol

: 77722-56-6
3-hydroxy-2,5-dimethyl-1-hexene

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent

2: 1.) magnesium, 5percent Cu(I)I / 1.) THF, -20 deg C, 30 min, 2.) overnight.

With copper(l) iodide; magnesium;
DOI:10.1007/BF00504391