Benzoic acid, 4-((2-furanyl((2-methyl-4-oxo-3(4H)-quinazolinyl)imino)methyl)azo)-, (phenylmethylene)hydrazide

Base Information

• Chemical Name: Benzoic acid, 4-((2-furanyl((2-methyl-4-oxo-3(4H)-quinazolinyl)imino)methyl)azo)-, (phenylmethylene)hydrazide
• CAS No.: 127786-20-3
• Molecular Formula: C28H21 N7 O3
• Molecular Weight: 503.5114
• Mol file: 127786-20-3.mol

Synonyms:BRN 3639133;127786-20-3;Benzoic acid, 4-((2-furanyl((2-methyl-4-oxo-3(4H)-quinazolinyl)imino)methyl)azo)-, (phenylmethylene)hydrazide;4-[(E)-{(Z)-2-Furyl[(2-methyl-4-oxo-3(4H)-quinazolinyl)imino]methyl}diazenyl]-N'-[(E)phenylmethylene]benzohydrazide;C28H21N7O3;C28-H21-N7-O3

Chemical Property of Benzoic acid, 4-((2-furanyl((2-methyl-4-oxo-3(4H)-quinazolinyl)imino)methyl)azo)-, (phenylmethylene)hydrazide

Chemical Property:

• XLogP3: 5
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 7
• Rotatable Bond Count: 7
• Exact Mass: 503.17058756
• Heavy Atom Count: 38
• Complexity: 964

Purity/Quality:

98%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=NC2=CC=CC=C2C(=O)N1N=C(C3=CC=CO3)N=NC4=CC=C(C=C4)C(=O)NN=CC5=CC=CC=C5
• Isomeric SMILES: CC1=NC2=CC=CC=C2C(=O)N1/N=C(/C3=CC=CO3)\N=NC4=CC=C(C=C4)C(=O)N/N=C/C5=CC=CC=C5

Technology Process of Benzoic acid, 4-((2-furanyl((2-methyl-4-oxo-3(4H)-quinazolinyl)imino)methyl)azo)-, (phenylmethylene)hydrazide

There total 4 articles about Benzoic acid, 4-((2-furanyl((2-methyl-4-oxo-3(4H)-quinazolinyl)imino)methyl)azo)-, (phenylmethylene)hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

4-<<<<2-methyl-4-oxo-3(4H)quinazolino>-imino>furfuryl>azo>benzoic acid hydrazide (127786-17-8) + benzaldehyde (100-52-7) → C28H21N7O3 (127786-20-3)

Guidance literature:

With acetic acid; In ethanol; for 5h; Heating;

DOI:10.1002/jps.2600790409

Reference yield:

2-methyl-3-(2-furylmethyleneamino)-quinazoline-(3H)-4-one (127786-15-6) → C28H21N7O3 (127786-20-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 60 percent / pyridine / Ambient temperature

2: 56 percent / glacial acetic acid / ethanol / 5 h / Heating

With pyridine; acetic acid; In ethanol;

DOI:10.1002/jps.2600790409

Reference yield:

4-Hydrazinocarbonyl-benzenediazonium; chloride (127786-26-9) → C28H21N7O3 (127786-20-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 60 percent / pyridine / Ambient temperature

2: 56 percent / glacial acetic acid / ethanol / 5 h / Heating

With pyridine; acetic acid; In ethanol;

DOI:10.1002/jps.2600790409

upstream raw materials:

4-<<<<2-methyl-4-oxo-3(4H)quinazolino>-imino>furfuryl>azo>benzoic acid hydrazide

benzaldehyde

2-methyl-3-(2-furylmethyleneamino)-quinazoline-(3H)-4-one

4-Hydrazinocarbonyl-benzenediazonium; chloride