1,3,4,6-Tetra-o-acetyl-2-deoxy-2-[(2,4-dinitrophenyl)amino]hexopyranose

Base Information

Chemical Name:1,3,4,6-Tetra-o-acetyl-2-deoxy-2-[(2,4-dinitrophenyl)amino]hexopyranose
CAS No.:7784-55-6
Molecular Formula:C20H23 N3 O13
Molecular Weight:513.415
Hs Code.:
NSC Number:409740,105408,105406
DSSTox Substance ID:DTXSID70295769,DTXSID80999049

Synonyms:10060-23-8;7784-55-6;1,3,4,6-tetra-o-acetyl-2-deoxy-2-[(2,4-dinitrophenyl)amino]hexopyranose;NSC105406;DTXSID70295769;DTXSID80999049;NSC105408;NSC409740;NSC-105406;NSC-105408;NSC-409740;1,3,4,6-Tetra-O-acetyl-2-deoxy-2-(2,4-dinitroanilino)hexopyranose

Suppliers and Price of 1,3,4,6-Tetra-o-acetyl-2-deoxy-2-[(2,4-dinitrophenyl)amino]hexopyranose

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 1,3,4,6-Tetra-o-acetyl-2-deoxy-2-[(2,4-dinitrophenyl)amino]hexopyranose

Chemical Property:

Vapor Pressure:8.42E-16mmHg at 25°C
Boiling Point:630.4°Cat760mmHg
Flash Point:335°C
Density:1.46g/cm³
XLogP3:1.7
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:14
Rotatable Bond Count:11
Exact Mass:513.12308780
Heavy Atom Count:36
Complexity:870

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=O)OCC1C(C(C(C(O1)OC(=O)C)NC2=C(C=C(C=C2)[N+](=O)[O-])[N+](=O)[O-])OC(=O)C)OC(=O)C

Technology Process of 1,3,4,6-Tetra-o-acetyl-2-deoxy-2-[(2,4-dinitrophenyl)amino]hexopyranose

There total 7 articles about 1,3,4,6-Tetra-o-acetyl-2-deoxy-2-[(2,4-dinitrophenyl)amino]hexopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7253-54-5
2-deoxy-2-(2,4-dinitro-phenyl)amino-D-glucose

: 108-24-7
acetic anhydride

: 7784-55-6
1,3,4,6-tetra-O-acetyl-2-deoxy-2-(2,4-dinitrophenylamino)-α-D-glucopyranose

Guidance literature:: With pyridine; at 20 ℃; for 1h;
DOI:10.1016/j.tetlet.2017.06.037

Reference yield:

: 7784-55-6,10060-23-8
Tetraacetyl-<2,4-dinitrophenyl>-glucosamin

Guidance literature:: N-<2,4-Dinitrophenyl>-d-glucosamin, Acetanhydrid, Py.;

Reference yield:

: 1078691-95-8
(+)-D-glucosamine hydrochloride

: 7784-55-6
1,3,4,6-tetra-O-acetyl-2-deoxy-2-(2,4-dinitrophenylamino)-α-D-glucopyranose

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / water; N,N-dimethyl-formamide / 2 h / 20 °C

2: pyridine / 1 h / 20 °C

With pyridine; triethylamine; In water; N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2017.06.037